Determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(II) chemiluminescence detection respectively

Asimple, rapid and sensitive method for the determination of psilocin and psilocybin is described. This is the first report on the determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bipyridyl)ruthenium(II) chemiluminescence. T...

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Main Authors: Anastos, N., Barnett, N., Lewis, Simon, Gathergood, N., Scammells, P., Sims, D.
Format: Journal Article
Published: Elsevier 2005
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/45369
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author Anastos, N.
Barnett, N.
Lewis, Simon
Gathergood, N.
Scammells, P.
Sims, D.
author_facet Anastos, N.
Barnett, N.
Lewis, Simon
Gathergood, N.
Scammells, P.
Sims, D.
author_sort Anastos, N.
building Curtin Institutional Repository
collection Online Access
description Asimple, rapid and sensitive method for the determination of psilocin and psilocybin is described. This is the first report on the determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bipyridyl)ruthenium(II) chemiluminescence. The limits of detection (signal-to-noise ratio = 3) are 9×10-10M and 3×10-10M for psilocin and psilocybin, respectively. A concise synthetic route for psilocin in three steps from readily available starting materials is also described. The structures were elucidated on the basis of spectroscopic data.
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institution Curtin University Malaysia
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publishDate 2005
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spelling curtin-20.500.11937-453692017-09-13T14:23:34Z Determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(II) chemiluminescence detection respectively Anastos, N. Barnett, N. Lewis, Simon Gathergood, N. Scammells, P. Sims, D. Psilocybin Psilocin Forensic analysis Synthesis Chemiluminescence Flow injection analysis Asimple, rapid and sensitive method for the determination of psilocin and psilocybin is described. This is the first report on the determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bipyridyl)ruthenium(II) chemiluminescence. The limits of detection (signal-to-noise ratio = 3) are 9×10-10M and 3×10-10M for psilocin and psilocybin, respectively. A concise synthetic route for psilocin in three steps from readily available starting materials is also described. The structures were elucidated on the basis of spectroscopic data. 2005 Journal Article http://hdl.handle.net/20.500.11937/45369 10.1016/j.talanta.2004.11.038 Elsevier restricted
spellingShingle Psilocybin
Psilocin
Forensic analysis
Synthesis
Chemiluminescence
Flow injection analysis
Anastos, N.
Barnett, N.
Lewis, Simon
Gathergood, N.
Scammells, P.
Sims, D.
Determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(II) chemiluminescence detection respectively
title Determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(II) chemiluminescence detection respectively
title_full Determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(II) chemiluminescence detection respectively
title_fullStr Determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(II) chemiluminescence detection respectively
title_full_unstemmed Determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(II) chemiluminescence detection respectively
title_short Determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(II) chemiluminescence detection respectively
title_sort determination of psilocin and psilocybin using flow injection analysis with acidic potassium permanganate and tris(2,2'-bypyridyl) ruthenium(ii) chemiluminescence detection respectively
topic Psilocybin
Psilocin
Forensic analysis
Synthesis
Chemiluminescence
Flow injection analysis
url http://hdl.handle.net/20.500.11937/45369