Quantum-sized BiVO4 modified TiO2 microflower composite heterostructures: Efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene

© The Royal Society of Chemistry 2015. In an effort to develop visible-light-driven heterostructured photocatalysts with high activity, a novel quantum-sized tubelike BiVO4 sensitized TiO2 microflower catalytic system was successfully fabricated by using a facile hydrothermal and ultrasonic adhering...

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Main Authors: Sun, J., Li, Xin Yong, Zhao, Q., Tadé, Moses, Liu, Shaomin
Format: Journal Article
Published: 2015
Online Access:http://hdl.handle.net/20.500.11937/44537
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author Sun, J.
Li, Xin Yong
Zhao, Q.
Tadé, Moses
Liu, Shaomin
author_facet Sun, J.
Li, Xin Yong
Zhao, Q.
Tadé, Moses
Liu, Shaomin
author_sort Sun, J.
building Curtin Institutional Repository
collection Online Access
description © The Royal Society of Chemistry 2015. In an effort to develop visible-light-driven heterostructured photocatalysts with high activity, a novel quantum-sized tubelike BiVO4 sensitized TiO2 microflower catalytic system was successfully fabricated by using a facile hydrothermal and ultrasonic adhering approach. The structural and optical properties of the as-prepared samples were comparatively characterized. The staggered band structure of quantum-sized BiVO4 decorated TiO2 not only extended the photo-response range but also promoted photoexcited charges transfer and separation. Photocatalytic activities of the as-prepared samples were examined by the degradation of toluene under visible light irradiation (? > 400 nm). Compared to the individual TiO2 microflower, BiVO4 quantum tube, BiVO4 nanoparticle and nano-BiVO4/TiO2, the quantum-BiVO4/TiO2 (Q-BiVO4/TiO2) composite exhibited higher photo activities. Electron spin resonance (ESR) examinations confirmed the generation of the photo-induced reactive oxygen species (OH and O2 -) which were involved in the photocatalytic process of Q-BiVO4/TiO2 composites. Furthermore, the enhanced photocatalytic activity of the Q-BiVO4/TiO2 composite mainly originated from the high separation efficiency of photo-induced electron-hole pairs and the efficient production of hydroxyl radicals. A detailed mechanism accounting for the superior photocatalytic activity was proposed in terms of the energy band structures of the components.
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spelling curtin-20.500.11937-445372017-09-13T14:14:26Z Quantum-sized BiVO4 modified TiO2 microflower composite heterostructures: Efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene Sun, J. Li, Xin Yong Zhao, Q. Tadé, Moses Liu, Shaomin © The Royal Society of Chemistry 2015. In an effort to develop visible-light-driven heterostructured photocatalysts with high activity, a novel quantum-sized tubelike BiVO4 sensitized TiO2 microflower catalytic system was successfully fabricated by using a facile hydrothermal and ultrasonic adhering approach. The structural and optical properties of the as-prepared samples were comparatively characterized. The staggered band structure of quantum-sized BiVO4 decorated TiO2 not only extended the photo-response range but also promoted photoexcited charges transfer and separation. Photocatalytic activities of the as-prepared samples were examined by the degradation of toluene under visible light irradiation (? > 400 nm). Compared to the individual TiO2 microflower, BiVO4 quantum tube, BiVO4 nanoparticle and nano-BiVO4/TiO2, the quantum-BiVO4/TiO2 (Q-BiVO4/TiO2) composite exhibited higher photo activities. Electron spin resonance (ESR) examinations confirmed the generation of the photo-induced reactive oxygen species (OH and O2 -) which were involved in the photocatalytic process of Q-BiVO4/TiO2 composites. Furthermore, the enhanced photocatalytic activity of the Q-BiVO4/TiO2 composite mainly originated from the high separation efficiency of photo-induced electron-hole pairs and the efficient production of hydroxyl radicals. A detailed mechanism accounting for the superior photocatalytic activity was proposed in terms of the energy band structures of the components. 2015 Journal Article http://hdl.handle.net/20.500.11937/44537 10.1039/c5ta05659d restricted
spellingShingle Sun, J.
Li, Xin Yong
Zhao, Q.
Tadé, Moses
Liu, Shaomin
Quantum-sized BiVO4 modified TiO2 microflower composite heterostructures: Efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene
title Quantum-sized BiVO4 modified TiO2 microflower composite heterostructures: Efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene
title_full Quantum-sized BiVO4 modified TiO2 microflower composite heterostructures: Efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene
title_fullStr Quantum-sized BiVO4 modified TiO2 microflower composite heterostructures: Efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene
title_full_unstemmed Quantum-sized BiVO4 modified TiO2 microflower composite heterostructures: Efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene
title_short Quantum-sized BiVO4 modified TiO2 microflower composite heterostructures: Efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene
title_sort quantum-sized bivo4 modified tio2 microflower composite heterostructures: efficient production of hydroxyl radicals towards visible light-driven degradation of gaseous toluene
url http://hdl.handle.net/20.500.11937/44537