Simultaneous ultra-trace palladium(II) detection and recovery from wastewater using new class meso-adsorbent

A novel functionalized mesoporous silica based meso-adsorbent was prepared for simple, efficient and rapid determination, sorption and recovery of trace palladium(II) in wastewater. The meso-adsorbent was prepared by indirect immobilization of ((3-(3-(methoxycarbonyl)benzylidene)hydrazinyl)benzoic a...

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Main Authors: Awual, M., Khaleque, M., Ratna, Y., Znad, Hussein
Format: Journal Article
Published: Elsevier 2015
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/44497
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author Awual, M.
Khaleque, M.
Ratna, Y.
Znad, Hussein
author_facet Awual, M.
Khaleque, M.
Ratna, Y.
Znad, Hussein
author_sort Awual, M.
building Curtin Institutional Repository
collection Online Access
description A novel functionalized mesoporous silica based meso-adsorbent was prepared for simple, efficient and rapid determination, sorption and recovery of trace palladium(II) in wastewater. The meso-adsorbent was prepared by indirect immobilization of ((3-(3-(methoxycarbonyl)benzylidene)hydrazinyl)benzoic acid) onto the cage-pored mesoporous silica. The optimum conditions were measured as a function of solution acidity, contact time, ion selectivity and adsorption isotherms models. The data revealed that meso-adsorbent offered simple and one-step procedure without using high tech instruments. The determined detection limit and sorption capacity were 0.11 μg/L and 184.50 mg/g, respectively. The meso-adsorbent can be repeatedly recycled without deterioration of the unique mesostructures and maintaining the same functionality for detection/sorption operations in next uses.
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institution Curtin University Malaysia
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publishDate 2015
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spelling curtin-20.500.11937-444972018-07-17T06:27:17Z Simultaneous ultra-trace palladium(II) detection and recovery from wastewater using new class meso-adsorbent Awual, M. Khaleque, M. Ratna, Y. Znad, Hussein Meso-adsorbent Selectivity and sensitivity Palladium(II) Reuses Detection and recovery A novel functionalized mesoporous silica based meso-adsorbent was prepared for simple, efficient and rapid determination, sorption and recovery of trace palladium(II) in wastewater. The meso-adsorbent was prepared by indirect immobilization of ((3-(3-(methoxycarbonyl)benzylidene)hydrazinyl)benzoic acid) onto the cage-pored mesoporous silica. The optimum conditions were measured as a function of solution acidity, contact time, ion selectivity and adsorption isotherms models. The data revealed that meso-adsorbent offered simple and one-step procedure without using high tech instruments. The determined detection limit and sorption capacity were 0.11 μg/L and 184.50 mg/g, respectively. The meso-adsorbent can be repeatedly recycled without deterioration of the unique mesostructures and maintaining the same functionality for detection/sorption operations in next uses. 2015 Journal Article http://hdl.handle.net/20.500.11937/44497 10.1016/j.jiec.2014.02.053 Elsevier restricted
spellingShingle Meso-adsorbent
Selectivity and sensitivity
Palladium(II)
Reuses
Detection and recovery
Awual, M.
Khaleque, M.
Ratna, Y.
Znad, Hussein
Simultaneous ultra-trace palladium(II) detection and recovery from wastewater using new class meso-adsorbent
title Simultaneous ultra-trace palladium(II) detection and recovery from wastewater using new class meso-adsorbent
title_full Simultaneous ultra-trace palladium(II) detection and recovery from wastewater using new class meso-adsorbent
title_fullStr Simultaneous ultra-trace palladium(II) detection and recovery from wastewater using new class meso-adsorbent
title_full_unstemmed Simultaneous ultra-trace palladium(II) detection and recovery from wastewater using new class meso-adsorbent
title_short Simultaneous ultra-trace palladium(II) detection and recovery from wastewater using new class meso-adsorbent
title_sort simultaneous ultra-trace palladium(ii) detection and recovery from wastewater using new class meso-adsorbent
topic Meso-adsorbent
Selectivity and sensitivity
Palladium(II)
Reuses
Detection and recovery
url http://hdl.handle.net/20.500.11937/44497