Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under visible light irradiation

Square-like B doped TiO2 nanocrystals were first synthesized by a mild solvothermal method with H3BO4 and titanium isopropoxide as the precursors, and isopropyl alcohol as reaction medium. Then, Ag nanoparticles were deposited on TiO2-B nanosquares by photo-deposition. The as-synthesized products ha...

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Main Authors: Yu, C., Wei, L., Li, Xin Yong, Chen, J., Fan, Q., Yu, J.
Format: Journal Article
Published: 2013
Online Access:http://hdl.handle.net/20.500.11937/43663
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author Yu, C.
Wei, L.
Li, Xin Yong
Chen, J.
Fan, Q.
Yu, J.
author_facet Yu, C.
Wei, L.
Li, Xin Yong
Chen, J.
Fan, Q.
Yu, J.
author_sort Yu, C.
building Curtin Institutional Repository
collection Online Access
description Square-like B doped TiO2 nanocrystals were first synthesized by a mild solvothermal method with H3BO4 and titanium isopropoxide as the precursors, and isopropyl alcohol as reaction medium. Then, Ag nanoparticles were deposited on TiO2-B nanosquares by photo-deposition. The as-synthesized products have been investigated by photocatalytic reaction test and characterized by powder X-ray diffraction (XRD), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), and UV-vis diffuse reflectance spectra (DRS). The results showed that boron was successfully doped into TiO2 nanosquares under solvothermal condition. The obtained Ag/TiO2-B composite showed high efficiency in degradation of acid orange II under visible light irradiation. The high photocatalytic performance could be attributed to the synergistic effect of B doping and the plasmon photocatalysis role of the deposited silver nanoparticles over TiO2. © 2013 Elsevier B.V. All rights reserved.
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spelling curtin-20.500.11937-436632017-09-13T13:38:56Z Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under visible light irradiation Yu, C. Wei, L. Li, Xin Yong Chen, J. Fan, Q. Yu, J. Square-like B doped TiO2 nanocrystals were first synthesized by a mild solvothermal method with H3BO4 and titanium isopropoxide as the precursors, and isopropyl alcohol as reaction medium. Then, Ag nanoparticles were deposited on TiO2-B nanosquares by photo-deposition. The as-synthesized products have been investigated by photocatalytic reaction test and characterized by powder X-ray diffraction (XRD), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), and UV-vis diffuse reflectance spectra (DRS). The results showed that boron was successfully doped into TiO2 nanosquares under solvothermal condition. The obtained Ag/TiO2-B composite showed high efficiency in degradation of acid orange II under visible light irradiation. The high photocatalytic performance could be attributed to the synergistic effect of B doping and the plasmon photocatalysis role of the deposited silver nanoparticles over TiO2. © 2013 Elsevier B.V. All rights reserved. 2013 Journal Article http://hdl.handle.net/20.500.11937/43663 10.1016/j.mseb.2013.01.015 restricted
spellingShingle Yu, C.
Wei, L.
Li, Xin Yong
Chen, J.
Fan, Q.
Yu, J.
Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under visible light irradiation
title Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under visible light irradiation
title_full Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under visible light irradiation
title_fullStr Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under visible light irradiation
title_full_unstemmed Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under visible light irradiation
title_short Synthesis and characterization of Ag/TiO2-B nanosquares with high photocatalytic activity under visible light irradiation
title_sort synthesis and characterization of ag/tio2-b nanosquares with high photocatalytic activity under visible light irradiation
url http://hdl.handle.net/20.500.11937/43663