Effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of Douglas fir wood

This paper investigates the effect of thermal pretreatment temperatures between 200 and 370 C on the yield and composition of products (bio-charm gasm water and organics) obtained when Douglas-fir wood was subsequently pyrolyzed in an auger reactor at 500 C. The yield of products was reported for th...

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Main Authors: Liaw, S., Zhou, S., Wu, Hongwei, Garcia-Perez, M.
Format: Journal Article
Published: Elsevier Science Ltd 2013
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/43444
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author Liaw, S.
Zhou, S.
Wu, Hongwei
Garcia-Perez, M.
author_facet Liaw, S.
Zhou, S.
Wu, Hongwei
Garcia-Perez, M.
author_sort Liaw, S.
building Curtin Institutional Repository
collection Online Access
description This paper investigates the effect of thermal pretreatment temperatures between 200 and 370 C on the yield and composition of products (bio-charm gasm water and organics) obtained when Douglas-fir wood was subsequently pyrolyzed in an auger reactor at 500 C. The yield of products was reported for the pretreatment and pyrolysis steps separately, and for the two steps added. The maximum yield of bio-oils achieved without pretreatment was close to 59 mass%. A decrease in total liquid yield was observed when the biomass was pretreated at 300 C. At higher temperatures, the yields of Douglas-fir primary degradation products (lignin oligomers, anhydrosugars and alkylated and methoxylated phenols) decreased. The overall water yield increased gradually to 14 mass% at a pretreatment temperature of 290 C. The yield of lignin oligomers also decreased as the pretreatment temperature increased. A drastic reduction in the yield of methoxylated phenols derived from guaiacyl (G) was observed when the biomass was pretreated at temperatures over 300 C. This drastic reduction in the yield of methoxylated lignin derivatives can be explained by the formation of liquid intermediates that facilitate the formation of ionic species, enhancing dehydration reactions leading to the production of o-quinone methide intermediates critical for bio-char formation.
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institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T09:16:15Z
publishDate 2013
publisher Elsevier Science Ltd
recordtype eprints
repository_type Digital Repository
spelling curtin-20.500.11937-434442017-02-28T01:44:34Z Effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of Douglas fir wood Liaw, S. Zhou, S. Wu, Hongwei Garcia-Perez, M. Torrefaction Douglas-fir Step-wise pyrolysis Bio-oil Auger pyrolysis This paper investigates the effect of thermal pretreatment temperatures between 200 and 370 C on the yield and composition of products (bio-charm gasm water and organics) obtained when Douglas-fir wood was subsequently pyrolyzed in an auger reactor at 500 C. The yield of products was reported for the pretreatment and pyrolysis steps separately, and for the two steps added. The maximum yield of bio-oils achieved without pretreatment was close to 59 mass%. A decrease in total liquid yield was observed when the biomass was pretreated at 300 C. At higher temperatures, the yields of Douglas-fir primary degradation products (lignin oligomers, anhydrosugars and alkylated and methoxylated phenols) decreased. The overall water yield increased gradually to 14 mass% at a pretreatment temperature of 290 C. The yield of lignin oligomers also decreased as the pretreatment temperature increased. A drastic reduction in the yield of methoxylated phenols derived from guaiacyl (G) was observed when the biomass was pretreated at temperatures over 300 C. This drastic reduction in the yield of methoxylated lignin derivatives can be explained by the formation of liquid intermediates that facilitate the formation of ionic species, enhancing dehydration reactions leading to the production of o-quinone methide intermediates critical for bio-char formation. 2013 Journal Article http://hdl.handle.net/20.500.11937/43444 Elsevier Science Ltd restricted
spellingShingle Torrefaction
Douglas-fir
Step-wise pyrolysis
Bio-oil
Auger pyrolysis
Liaw, S.
Zhou, S.
Wu, Hongwei
Garcia-Perez, M.
Effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of Douglas fir wood
title Effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of Douglas fir wood
title_full Effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of Douglas fir wood
title_fullStr Effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of Douglas fir wood
title_full_unstemmed Effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of Douglas fir wood
title_short Effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of Douglas fir wood
title_sort effect of pretreatment temperature on the yield and properties of bio-oils obtained from the auger pyrolysis of douglas fir wood
topic Torrefaction
Douglas-fir
Step-wise pyrolysis
Bio-oil
Auger pyrolysis
url http://hdl.handle.net/20.500.11937/43444