Correlation between polymer packing and gas transport properties for CO2/N2 separation in glassy fluorinated polyimide membrane

Gas separation performance of a membrane highly hinges on its physical properties. In this study, the interplay between polymer packing of a membrane and its gas transport behaviours (permeability and selectivity) was investigated through a series of 6FDA-DAM:DABA (3:2) polyimide membranes with diff...

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Main Author: Jawad, Zeinab
Format: Journal Article
Published: School of Engineering, Taylor’s University 2016
Online Access:http://jestec.taylors.edu.my/Vol%2011%20issue%207%20July%202016/11_7_2.pdf
http://hdl.handle.net/20.500.11937/43075
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author Jawad, Zeinab
author_facet Jawad, Zeinab
author_sort Jawad, Zeinab
building Curtin Institutional Repository
collection Online Access
description Gas separation performance of a membrane highly hinges on its physical properties. In this study, the interplay between polymer packing of a membrane and its gas transport behaviours (permeability and selectivity) was investigated through a series of 6FDA-DAM:DABA (3:2) polyimide membranes with different polymer compactness. The chemical structure and the polymer packing of the resulting membrane were characterized using attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) and packing density measurement, respectively. CO2/N2 separation efficiency of the membrane was evaluated at 25°C with feed pressure up to 6 bar. N2 permeability was found to rely on the membrane’s packing density, which signified its greater dependence on molecular sieving. In contrast, sorption showed a more vital role in determining the CO2 permeability. In this work, the membrane with a final thickness of 97±2 μm had successfully surpassed the Robeson’s 2008 upper bound plot with a CO2 permeability of 83 Barrer and CO2/N2 selectivity of 97 at 3 bar permeation.
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spelling curtin-20.500.11937-430752017-01-30T15:04:29Z Correlation between polymer packing and gas transport properties for CO2/N2 separation in glassy fluorinated polyimide membrane Jawad, Zeinab Gas separation performance of a membrane highly hinges on its physical properties. In this study, the interplay between polymer packing of a membrane and its gas transport behaviours (permeability and selectivity) was investigated through a series of 6FDA-DAM:DABA (3:2) polyimide membranes with different polymer compactness. The chemical structure and the polymer packing of the resulting membrane were characterized using attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) and packing density measurement, respectively. CO2/N2 separation efficiency of the membrane was evaluated at 25°C with feed pressure up to 6 bar. N2 permeability was found to rely on the membrane’s packing density, which signified its greater dependence on molecular sieving. In contrast, sorption showed a more vital role in determining the CO2 permeability. In this work, the membrane with a final thickness of 97±2 μm had successfully surpassed the Robeson’s 2008 upper bound plot with a CO2 permeability of 83 Barrer and CO2/N2 selectivity of 97 at 3 bar permeation. 2016 Journal Article http://hdl.handle.net/20.500.11937/43075 http://jestec.taylors.edu.my/Vol%2011%20issue%207%20July%202016/11_7_2.pdf School of Engineering, Taylor’s University restricted
spellingShingle Jawad, Zeinab
Correlation between polymer packing and gas transport properties for CO2/N2 separation in glassy fluorinated polyimide membrane
title Correlation between polymer packing and gas transport properties for CO2/N2 separation in glassy fluorinated polyimide membrane
title_full Correlation between polymer packing and gas transport properties for CO2/N2 separation in glassy fluorinated polyimide membrane
title_fullStr Correlation between polymer packing and gas transport properties for CO2/N2 separation in glassy fluorinated polyimide membrane
title_full_unstemmed Correlation between polymer packing and gas transport properties for CO2/N2 separation in glassy fluorinated polyimide membrane
title_short Correlation between polymer packing and gas transport properties for CO2/N2 separation in glassy fluorinated polyimide membrane
title_sort correlation between polymer packing and gas transport properties for co2/n2 separation in glassy fluorinated polyimide membrane
url http://jestec.taylors.edu.my/Vol%2011%20issue%207%20July%202016/11_7_2.pdf
http://hdl.handle.net/20.500.11937/43075