Facile synthesis of sub-monolayer Sn, Ru, and RuSn decorated Pt/C nanoparticles for formaldehyde electrooxidation

A novel structured catalyst for formaldehyde electrooxidation was developed by decorating sub-monolayer Sn, Ru and RuSn on the surface of Pt/C nanoparticles. The electrocatalysts were prepared by an impregnation-reduction method using H2 as the reducing agent at room temperature. The structure and e...

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Main Authors: Wang, D., Wang, J., Lu, S., Jiang, San Ping
Format: Journal Article
Published: Elsevier 2014
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/42573
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author Wang, D.
Wang, J.
Lu, S.
Jiang, San Ping
author_facet Wang, D.
Wang, J.
Lu, S.
Jiang, San Ping
author_sort Wang, D.
building Curtin Institutional Repository
collection Online Access
description A novel structured catalyst for formaldehyde electrooxidation was developed by decorating sub-monolayer Sn, Ru and RuSn on the surface of Pt/C nanoparticles. The electrocatalysts were prepared by an impregnation-reduction method using H2 as the reducing agent at room temperature. The structure and electrochemical active surface area of the decorated Pt/C electrocatalysts were characterized by Xray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), energy dispersion spectroscopy (EDX) and cyclic voltammetry (CV). High electrocatalytic activities of Sn, Ru and RuSn decorated Pt/C electrodes toward formaldehyde electrooxidation in a 0.5 M H2SO4 aqueous solution were observed as compared with pure Pt/C electrode. Best results were obtained on the Sn decorated Pt/C electrocatalyst with a significantly lower onset potential and higher oxidation current in acid medium, relative to the pure Pt/C and Ru decorated Pt/C electrocatalysts. The reasons are most likely related to the fact that Sn, existed as tin oxides, has significantly higher activation and catalytic activity towards CO oxidation and the presence of Sn induces the weakly bonded CO on Pt.
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institution Curtin University Malaysia
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publishDate 2014
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spelling curtin-20.500.11937-425732017-09-13T15:57:41Z Facile synthesis of sub-monolayer Sn, Ru, and RuSn decorated Pt/C nanoparticles for formaldehyde electrooxidation Wang, D. Wang, J. Lu, S. Jiang, San Ping Ru decorated Pt nanoparticles - CO stripping Sn decorated Pt nanoparticles Fuel cells Formaldehyde oxidation A novel structured catalyst for formaldehyde electrooxidation was developed by decorating sub-monolayer Sn, Ru and RuSn on the surface of Pt/C nanoparticles. The electrocatalysts were prepared by an impregnation-reduction method using H2 as the reducing agent at room temperature. The structure and electrochemical active surface area of the decorated Pt/C electrocatalysts were characterized by Xray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), energy dispersion spectroscopy (EDX) and cyclic voltammetry (CV). High electrocatalytic activities of Sn, Ru and RuSn decorated Pt/C electrodes toward formaldehyde electrooxidation in a 0.5 M H2SO4 aqueous solution were observed as compared with pure Pt/C electrode. Best results were obtained on the Sn decorated Pt/C electrocatalyst with a significantly lower onset potential and higher oxidation current in acid medium, relative to the pure Pt/C and Ru decorated Pt/C electrocatalysts. The reasons are most likely related to the fact that Sn, existed as tin oxides, has significantly higher activation and catalytic activity towards CO oxidation and the presence of Sn induces the weakly bonded CO on Pt. 2014 Journal Article http://hdl.handle.net/20.500.11937/42573 10.1016/j.jelechem.2013.10.008 Elsevier restricted
spellingShingle Ru decorated Pt nanoparticles - CO stripping
Sn decorated Pt nanoparticles
Fuel cells
Formaldehyde oxidation
Wang, D.
Wang, J.
Lu, S.
Jiang, San Ping
Facile synthesis of sub-monolayer Sn, Ru, and RuSn decorated Pt/C nanoparticles for formaldehyde electrooxidation
title Facile synthesis of sub-monolayer Sn, Ru, and RuSn decorated Pt/C nanoparticles for formaldehyde electrooxidation
title_full Facile synthesis of sub-monolayer Sn, Ru, and RuSn decorated Pt/C nanoparticles for formaldehyde electrooxidation
title_fullStr Facile synthesis of sub-monolayer Sn, Ru, and RuSn decorated Pt/C nanoparticles for formaldehyde electrooxidation
title_full_unstemmed Facile synthesis of sub-monolayer Sn, Ru, and RuSn decorated Pt/C nanoparticles for formaldehyde electrooxidation
title_short Facile synthesis of sub-monolayer Sn, Ru, and RuSn decorated Pt/C nanoparticles for formaldehyde electrooxidation
title_sort facile synthesis of sub-monolayer sn, ru, and rusn decorated pt/c nanoparticles for formaldehyde electrooxidation
topic Ru decorated Pt nanoparticles - CO stripping
Sn decorated Pt nanoparticles
Fuel cells
Formaldehyde oxidation
url http://hdl.handle.net/20.500.11937/42573