Graphene Oxide Sheathed ZIF-8 Microcrystals: Engineered Precursors of Nitrogen-Doped Porous Carbon for Efficient Oxygen Reduction Reaction (ORR) Electrocatalysis

© 2016 American Chemical Society.Nitrogen containing mesoporous carbon obtained by the pyrolysis of graphene oxide (GO) wrapped ZIF-8 (Zeolitic Imidazolate Frameworks-8) micro crystals is demonstrated to be an efficient catalyst for the oxygen reduction reaction (ORR). ZIF-8 synthesis in the presenc...

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Main Authors: Thomas, M., Illathvalappil, R., Kurungot, S., Nair, Balagopal, Mohamed, A., Anilkumar, G., Yamaguchi, T., Hareesh, U.
Format: Journal Article
Published: American Chemical Society 2016
Online Access:http://hdl.handle.net/20.500.11937/42449
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author Thomas, M.
Illathvalappil, R.
Kurungot, S.
Nair, Balagopal
Mohamed, A.
Anilkumar, G.
Yamaguchi, T.
Hareesh, U.
author_facet Thomas, M.
Illathvalappil, R.
Kurungot, S.
Nair, Balagopal
Mohamed, A.
Anilkumar, G.
Yamaguchi, T.
Hareesh, U.
author_sort Thomas, M.
building Curtin Institutional Repository
collection Online Access
description © 2016 American Chemical Society.Nitrogen containing mesoporous carbon obtained by the pyrolysis of graphene oxide (GO) wrapped ZIF-8 (Zeolitic Imidazolate Frameworks-8) micro crystals is demonstrated to be an efficient catalyst for the oxygen reduction reaction (ORR). ZIF-8 synthesis in the presence of GO sheets helped to realize layers of graphene oxide over ZIF-8 microcrystals and the sphere-like structures thus obtained, on heat treatment, transformed to highly porous carbon with a nitrogen content of about 6.12% and surface area of 502 m2/g. These catalysts with a typical micromeso porous architecture exhibited an onset potential of 0.88Vvs RHE in a four electron pathway and also demonstrated superior durability in alkaline medium compared to that of the commercial Pt/C catalyst. The N-doped porous carbon derived from GO sheathed ZIF-8 core-shell structures could therefore be employed as an efficient electrocatalyst for fuel cell applications.
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institution Curtin University Malaysia
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publishDate 2016
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spelling curtin-20.500.11937-424492017-09-13T14:25:26Z Graphene Oxide Sheathed ZIF-8 Microcrystals: Engineered Precursors of Nitrogen-Doped Porous Carbon for Efficient Oxygen Reduction Reaction (ORR) Electrocatalysis Thomas, M. Illathvalappil, R. Kurungot, S. Nair, Balagopal Mohamed, A. Anilkumar, G. Yamaguchi, T. Hareesh, U. © 2016 American Chemical Society.Nitrogen containing mesoporous carbon obtained by the pyrolysis of graphene oxide (GO) wrapped ZIF-8 (Zeolitic Imidazolate Frameworks-8) micro crystals is demonstrated to be an efficient catalyst for the oxygen reduction reaction (ORR). ZIF-8 synthesis in the presence of GO sheets helped to realize layers of graphene oxide over ZIF-8 microcrystals and the sphere-like structures thus obtained, on heat treatment, transformed to highly porous carbon with a nitrogen content of about 6.12% and surface area of 502 m2/g. These catalysts with a typical micromeso porous architecture exhibited an onset potential of 0.88Vvs RHE in a four electron pathway and also demonstrated superior durability in alkaline medium compared to that of the commercial Pt/C catalyst. The N-doped porous carbon derived from GO sheathed ZIF-8 core-shell structures could therefore be employed as an efficient electrocatalyst for fuel cell applications. 2016 Journal Article http://hdl.handle.net/20.500.11937/42449 10.1021/acsami.6b06979 American Chemical Society restricted
spellingShingle Thomas, M.
Illathvalappil, R.
Kurungot, S.
Nair, Balagopal
Mohamed, A.
Anilkumar, G.
Yamaguchi, T.
Hareesh, U.
Graphene Oxide Sheathed ZIF-8 Microcrystals: Engineered Precursors of Nitrogen-Doped Porous Carbon for Efficient Oxygen Reduction Reaction (ORR) Electrocatalysis
title Graphene Oxide Sheathed ZIF-8 Microcrystals: Engineered Precursors of Nitrogen-Doped Porous Carbon for Efficient Oxygen Reduction Reaction (ORR) Electrocatalysis
title_full Graphene Oxide Sheathed ZIF-8 Microcrystals: Engineered Precursors of Nitrogen-Doped Porous Carbon for Efficient Oxygen Reduction Reaction (ORR) Electrocatalysis
title_fullStr Graphene Oxide Sheathed ZIF-8 Microcrystals: Engineered Precursors of Nitrogen-Doped Porous Carbon for Efficient Oxygen Reduction Reaction (ORR) Electrocatalysis
title_full_unstemmed Graphene Oxide Sheathed ZIF-8 Microcrystals: Engineered Precursors of Nitrogen-Doped Porous Carbon for Efficient Oxygen Reduction Reaction (ORR) Electrocatalysis
title_short Graphene Oxide Sheathed ZIF-8 Microcrystals: Engineered Precursors of Nitrogen-Doped Porous Carbon for Efficient Oxygen Reduction Reaction (ORR) Electrocatalysis
title_sort graphene oxide sheathed zif-8 microcrystals: engineered precursors of nitrogen-doped porous carbon for efficient oxygen reduction reaction (orr) electrocatalysis
url http://hdl.handle.net/20.500.11937/42449