The effect of a copolymer inhibitor on baryte precipitation

In situ atomic force microscopy (AFM) experiments were used to study the effect of trace amounts of a commercial inhibitor on the (001) baryte surface during growth. The additive tested was a copolymer, used as a scale inhibitor in oil recovery (maleic acid/allyl sulfonic acid copolymer with phospho...

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Main Authors: Ruiz-Agudo, C., Putnis, Christine, Putnis, Andrew
Format: Journal Article
Published: Mineralogical Society 2014
Online Access:http://hdl.handle.net/20.500.11937/42406
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author Ruiz-Agudo, C.
Putnis, Christine
Putnis, Andrew
author_facet Ruiz-Agudo, C.
Putnis, Christine
Putnis, Andrew
author_sort Ruiz-Agudo, C.
building Curtin Institutional Repository
collection Online Access
description In situ atomic force microscopy (AFM) experiments were used to study the effect of trace amounts of a commercial inhibitor on the (001) baryte surface during growth. The additive tested was a copolymer, used as a scale inhibitor in oil recovery (maleic acid/allyl sulfonic acid copolymer with phosphonate groups, partial sodium salt). The morphology of the growth was used to gain a better understanding of the inhibition mechanism. Without an inhibitor, barium sulfate growth occurred by 2D island nucleation and spreading. The addition of a small amount (0.1 ppm and 0.5 ppm) of copolymer inhibitor enhances 2D nucleation but blocks growth. Just 1 ppm of inhibitor blocks nucleation and growth by adsorption of a copolymer layer onto the baryte surface. Similarly in 3D studies, small amounts of inhibitor seem to act on growth and not on nucleation and larger amounts of copolymer act on both by adsorption of the copolymer to all baryte surfaces keeping the particles in their embryo stage.
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spelling curtin-20.500.11937-424062017-09-13T14:26:11Z The effect of a copolymer inhibitor on baryte precipitation Ruiz-Agudo, C. Putnis, Christine Putnis, Andrew In situ atomic force microscopy (AFM) experiments were used to study the effect of trace amounts of a commercial inhibitor on the (001) baryte surface during growth. The additive tested was a copolymer, used as a scale inhibitor in oil recovery (maleic acid/allyl sulfonic acid copolymer with phosphonate groups, partial sodium salt). The morphology of the growth was used to gain a better understanding of the inhibition mechanism. Without an inhibitor, barium sulfate growth occurred by 2D island nucleation and spreading. The addition of a small amount (0.1 ppm and 0.5 ppm) of copolymer inhibitor enhances 2D nucleation but blocks growth. Just 1 ppm of inhibitor blocks nucleation and growth by adsorption of a copolymer layer onto the baryte surface. Similarly in 3D studies, small amounts of inhibitor seem to act on growth and not on nucleation and larger amounts of copolymer act on both by adsorption of the copolymer to all baryte surfaces keeping the particles in their embryo stage. 2014 Journal Article http://hdl.handle.net/20.500.11937/42406 10.1180/minmag.2014.078.6.09 Mineralogical Society restricted
spellingShingle Ruiz-Agudo, C.
Putnis, Christine
Putnis, Andrew
The effect of a copolymer inhibitor on baryte precipitation
title The effect of a copolymer inhibitor on baryte precipitation
title_full The effect of a copolymer inhibitor on baryte precipitation
title_fullStr The effect of a copolymer inhibitor on baryte precipitation
title_full_unstemmed The effect of a copolymer inhibitor on baryte precipitation
title_short The effect of a copolymer inhibitor on baryte precipitation
title_sort effect of a copolymer inhibitor on baryte precipitation
url http://hdl.handle.net/20.500.11937/42406