Effect of solution parameters on electrospun PLA/PCL fibers

This research work focused on studying two different concentrations of poly (ε-caprolactone) (PCL) and blends of PCL with Poly (lactic acid) (PLA) at five blending rations and that are dissolved in different co-solvents (chloroform: methanol and dichloromethane (DCM) : N,N, dimethylformamide (DMF))....

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Main Authors: Haroosh, Hazim, Chaudhary, Deeptangshu, Dong, Yu
Other Authors: Rose Amal
Format: Conference Paper
Published: UNSW 2011
Online Access:http://hdl.handle.net/20.500.11937/42070
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author Haroosh, Hazim
Chaudhary, Deeptangshu
Dong, Yu
author2 Rose Amal
author_facet Rose Amal
Haroosh, Hazim
Chaudhary, Deeptangshu
Dong, Yu
author_sort Haroosh, Hazim
building Curtin Institutional Repository
collection Online Access
description This research work focused on studying two different concentrations of poly (ε-caprolactone) (PCL) and blends of PCL with Poly (lactic acid) (PLA) at five blending rations and that are dissolved in different co-solvents (chloroform: methanol and dichloromethane (DCM) : N,N, dimethylformamide (DMF)). The fibers produced from the DCM:DMF system for all percentages of polymer blends were smaller in fiber diameter as compared to the fibers produced from the chloroform: methanol system. However, it was found that generally, the fiber properties were related to the viscosity and conductivity of their bulk solution. The fiber diameters and the surface morphology were dependent on the PLA/PCL ratio and also on the relevant co-solvent amount. Solution concentration, viscosity, conductivity and solvent volatility were found to be the key factors that controlled the fiber diameter. In addition, the chain entanglements in the solution and the dielectric constant of the solvent have a significant influence on the morphology of the resulting fibers. Furthermore, increasing the PCL amount in blends increased the solution viscosity, and higher viscosity led to electrospun fibers with larger diameters.
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institution Curtin University Malaysia
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spelling curtin-20.500.11937-420702023-01-27T05:52:11Z Effect of solution parameters on electrospun PLA/PCL fibers Haroosh, Hazim Chaudhary, Deeptangshu Dong, Yu Rose Amal Vincent Gomes Vicki Chen This research work focused on studying two different concentrations of poly (ε-caprolactone) (PCL) and blends of PCL with Poly (lactic acid) (PLA) at five blending rations and that are dissolved in different co-solvents (chloroform: methanol and dichloromethane (DCM) : N,N, dimethylformamide (DMF)). The fibers produced from the DCM:DMF system for all percentages of polymer blends were smaller in fiber diameter as compared to the fibers produced from the chloroform: methanol system. However, it was found that generally, the fiber properties were related to the viscosity and conductivity of their bulk solution. The fiber diameters and the surface morphology were dependent on the PLA/PCL ratio and also on the relevant co-solvent amount. Solution concentration, viscosity, conductivity and solvent volatility were found to be the key factors that controlled the fiber diameter. In addition, the chain entanglements in the solution and the dielectric constant of the solvent have a significant influence on the morphology of the resulting fibers. Furthermore, increasing the PCL amount in blends increased the solution viscosity, and higher viscosity led to electrospun fibers with larger diameters. 2011 Conference Paper http://hdl.handle.net/20.500.11937/42070 UNSW restricted
spellingShingle Haroosh, Hazim
Chaudhary, Deeptangshu
Dong, Yu
Effect of solution parameters on electrospun PLA/PCL fibers
title Effect of solution parameters on electrospun PLA/PCL fibers
title_full Effect of solution parameters on electrospun PLA/PCL fibers
title_fullStr Effect of solution parameters on electrospun PLA/PCL fibers
title_full_unstemmed Effect of solution parameters on electrospun PLA/PCL fibers
title_short Effect of solution parameters on electrospun PLA/PCL fibers
title_sort effect of solution parameters on electrospun pla/pcl fibers
url http://hdl.handle.net/20.500.11937/42070