Comparative investigation of photocatalytic degradation of toluene on Nitrogen doped Ta2O5 and Nb2O5 nanoparticles

Nb2O5 and Ta2O5 nanoparticles were prepared at a moderate sintering temperature of 700 °C using a solution method. Nitrogen doped Nb2O5 and Ta2O5 were obtained by ammonia gas treatment at 700 °C. The materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier...

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Main Authors: Ullah, Ruh, Sun, Hongqi, Ang, Ha Ming, Tade, Moses, Wang, Shaobin
Format: Journal Article
Published: American Chemical Society 2013
Online Access:http://hdl.handle.net/20.500.11937/40856
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author Ullah, Ruh
Sun, Hongqi
Ang, Ha Ming
Tade, Moses
Wang, Shaobin
author_facet Ullah, Ruh
Sun, Hongqi
Ang, Ha Ming
Tade, Moses
Wang, Shaobin
author_sort Ullah, Ruh
building Curtin Institutional Repository
collection Online Access
description Nb2O5 and Ta2O5 nanoparticles were prepared at a moderate sintering temperature of 700 °C using a solution method. Nitrogen doped Nb2O5 and Ta2O5 were obtained by ammonia gas treatment at 700 °C. The materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), and UV-vis diffuse reflectance spectroscopy. All the materials were used for photocatalytic decomposition of gaseous toluene irradiated with artificial solar light and pure visible light. Most of the materials were multiple crystallites with orthorhombic and monoclinic structures. Tantalum based compounds, undoped (Ta2O5 (lab)) and nitrogen doped (Ta2O5:N (lab)), have shown much better performance than niobium based materials. Ta2O5:N (lab) decomposed gaseous toluene with a rate similar to those of Ta2O5 (lab) and Ta2O5:N (com) in the initial 60 min but at a higher rate at extended time under artificial sunlight. Ta2O5:N (lab) decomposed about 70% toluene with artificial sunlight and 30% with pure visible light (lambda = 400 nm). The material also exhibited a very stable performance with artificial sunlight and pure visible light.
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publishDate 2013
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spelling curtin-20.500.11937-408562017-09-13T14:03:54Z Comparative investigation of photocatalytic degradation of toluene on Nitrogen doped Ta2O5 and Nb2O5 nanoparticles Ullah, Ruh Sun, Hongqi Ang, Ha Ming Tade, Moses Wang, Shaobin Nb2O5 and Ta2O5 nanoparticles were prepared at a moderate sintering temperature of 700 °C using a solution method. Nitrogen doped Nb2O5 and Ta2O5 were obtained by ammonia gas treatment at 700 °C. The materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), and UV-vis diffuse reflectance spectroscopy. All the materials were used for photocatalytic decomposition of gaseous toluene irradiated with artificial solar light and pure visible light. Most of the materials were multiple crystallites with orthorhombic and monoclinic structures. Tantalum based compounds, undoped (Ta2O5 (lab)) and nitrogen doped (Ta2O5:N (lab)), have shown much better performance than niobium based materials. Ta2O5:N (lab) decomposed gaseous toluene with a rate similar to those of Ta2O5 (lab) and Ta2O5:N (com) in the initial 60 min but at a higher rate at extended time under artificial sunlight. Ta2O5:N (lab) decomposed about 70% toluene with artificial sunlight and 30% with pure visible light (lambda = 400 nm). The material also exhibited a very stable performance with artificial sunlight and pure visible light. 2013 Journal Article http://hdl.handle.net/20.500.11937/40856 10.1021/ie302326h American Chemical Society restricted
spellingShingle Ullah, Ruh
Sun, Hongqi
Ang, Ha Ming
Tade, Moses
Wang, Shaobin
Comparative investigation of photocatalytic degradation of toluene on Nitrogen doped Ta2O5 and Nb2O5 nanoparticles
title Comparative investigation of photocatalytic degradation of toluene on Nitrogen doped Ta2O5 and Nb2O5 nanoparticles
title_full Comparative investigation of photocatalytic degradation of toluene on Nitrogen doped Ta2O5 and Nb2O5 nanoparticles
title_fullStr Comparative investigation of photocatalytic degradation of toluene on Nitrogen doped Ta2O5 and Nb2O5 nanoparticles
title_full_unstemmed Comparative investigation of photocatalytic degradation of toluene on Nitrogen doped Ta2O5 and Nb2O5 nanoparticles
title_short Comparative investigation of photocatalytic degradation of toluene on Nitrogen doped Ta2O5 and Nb2O5 nanoparticles
title_sort comparative investigation of photocatalytic degradation of toluene on nitrogen doped ta2o5 and nb2o5 nanoparticles
url http://hdl.handle.net/20.500.11937/40856