Microstructual Design of Lead Oxide-Epoxy Composites for Radiation Shielding Purposes

Composite epoxy samples filled with PbO and Pb3O4 were fabricated to investigate the mass attenuation characteristics of the composites to X-rays in the diagnostic imaging energy range. The effect of density on the attenuation ability of the composites for radiation shielding purposes was studied us...

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Main Authors: Noor Azman, N., Siddiqui, Salim, Hart, Robin, Low, It-Meng (Jim)
Format: Journal Article
Published: John Wiley and Sons Inc 2012
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/40358
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author Noor Azman, N.
Siddiqui, Salim
Hart, Robin
Low, It-Meng (Jim)
author_facet Noor Azman, N.
Siddiqui, Salim
Hart, Robin
Low, It-Meng (Jim)
author_sort Noor Azman, N.
building Curtin Institutional Repository
collection Online Access
description Composite epoxy samples filled with PbO and Pb3O4 were fabricated to investigate the mass attenuation characteristics of the composites to X-rays in the diagnostic imaging energy range. The effect of density on the attenuation ability of the composites for radiation shielding purposes was studied using a calibrated X-ray machine. Characterization of the microstructure properties of the synthesized composites was performed using synchrotron radiation diffraction, optical microscopy, and scanning electron microscopy. The results indicate that the attenuation ability of the composites increased with an increase in density. The particle size of WO3 fillers has a negligible effect on the value of mass attenuation coefficient. Microstructural analyses have confirmed the existence of fairly uniform dispersion of fillers within the matrix of epoxy matrix with the average particle size of 1–5 μm for composites with filler loading of ≤ 30 wt % and 5–15 μm for composites with filler loading of ≥ 50 wt %.
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institution Curtin University Malaysia
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publishDate 2012
publisher John Wiley and Sons Inc
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spelling curtin-20.500.11937-403582019-02-19T04:27:51Z Microstructual Design of Lead Oxide-Epoxy Composites for Radiation Shielding Purposes Noor Azman, N. Siddiqui, Salim Hart, Robin Low, It-Meng (Jim) radiation density resins microscopy composites Composite epoxy samples filled with PbO and Pb3O4 were fabricated to investigate the mass attenuation characteristics of the composites to X-rays in the diagnostic imaging energy range. The effect of density on the attenuation ability of the composites for radiation shielding purposes was studied using a calibrated X-ray machine. Characterization of the microstructure properties of the synthesized composites was performed using synchrotron radiation diffraction, optical microscopy, and scanning electron microscopy. The results indicate that the attenuation ability of the composites increased with an increase in density. The particle size of WO3 fillers has a negligible effect on the value of mass attenuation coefficient. Microstructural analyses have confirmed the existence of fairly uniform dispersion of fillers within the matrix of epoxy matrix with the average particle size of 1–5 μm for composites with filler loading of ≤ 30 wt % and 5–15 μm for composites with filler loading of ≥ 50 wt %. 2012 Journal Article http://hdl.handle.net/20.500.11937/40358 10.1002/app.38515 John Wiley and Sons Inc restricted
spellingShingle radiation
density
resins
microscopy
composites
Noor Azman, N.
Siddiqui, Salim
Hart, Robin
Low, It-Meng (Jim)
Microstructual Design of Lead Oxide-Epoxy Composites for Radiation Shielding Purposes
title Microstructual Design of Lead Oxide-Epoxy Composites for Radiation Shielding Purposes
title_full Microstructual Design of Lead Oxide-Epoxy Composites for Radiation Shielding Purposes
title_fullStr Microstructual Design of Lead Oxide-Epoxy Composites for Radiation Shielding Purposes
title_full_unstemmed Microstructual Design of Lead Oxide-Epoxy Composites for Radiation Shielding Purposes
title_short Microstructual Design of Lead Oxide-Epoxy Composites for Radiation Shielding Purposes
title_sort microstructual design of lead oxide-epoxy composites for radiation shielding purposes
topic radiation
density
resins
microscopy
composites
url http://hdl.handle.net/20.500.11937/40358