Effect of a reducing agent for silver on the electrochemical activity of an Ag/Ba0.5Sr0.5Co0.8Fe0.2O3-d electrode prepared by electroless deposition technique

Silver-modified Ba0.5Sr0.5Co0.8Fe0.2O3-d (Ag/BSCF) electrodes were prepared using an electroless deposition technique. The morphology, microstructure and oxygen reduction reaction activity of the resulted Ag/BSCF electrodes were comparatively studied using Fourier transform infrared spectra, environ...

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Main Authors: Zhou, W., Ran, R., Cai, R., Shao, Zongping, Jin, W., Xu, N.
Format: Journal Article
Published: Elsevier SA 2009
Online Access:http://hdl.handle.net/20.500.11937/39000
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author Zhou, W.
Ran, R.
Cai, R.
Shao, Zongping
Jin, W.
Xu, N.
author_facet Zhou, W.
Ran, R.
Cai, R.
Shao, Zongping
Jin, W.
Xu, N.
author_sort Zhou, W.
building Curtin Institutional Repository
collection Online Access
description Silver-modified Ba0.5Sr0.5Co0.8Fe0.2O3-d (Ag/BSCF) electrodes were prepared using an electroless deposition technique. The morphology, microstructure and oxygen reduction reaction activity of the resulted Ag/BSCF electrodes were comparatively studied using Fourier transform infrared spectra, environmental scanning electron microscopy, temperature-programmed oxygen desorption, X-ray diffraction, and electrochemical impedance spectroscopy. An area-specific resistance as low as 0.038 O cm2 was achieved for N2H4-reduced Ag/BSCF cathode at 600 °C. Carbonates were detected over the BSCF surface during the reduction of silver, which deteriorated both the charge-transfer process and diffusion process of HCHO-reduced Ag/BSCF cathode for the oxygen electrochemical reduction reaction. An anode-supported single cell with an N2H4-reduced Ag/BSCF cathode showed a peak power of 826 mW cm-2 at 600 °C. In comparison, only 672 mW cm-2 was observed with the HCHO-reduced Ag/BSCF cathode. © 2008 Elsevier B.V. All rights reserved.
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spelling curtin-20.500.11937-390002017-09-13T14:20:16Z Effect of a reducing agent for silver on the electrochemical activity of an Ag/Ba0.5Sr0.5Co0.8Fe0.2O3-d electrode prepared by electroless deposition technique Zhou, W. Ran, R. Cai, R. Shao, Zongping Jin, W. Xu, N. Silver-modified Ba0.5Sr0.5Co0.8Fe0.2O3-d (Ag/BSCF) electrodes were prepared using an electroless deposition technique. The morphology, microstructure and oxygen reduction reaction activity of the resulted Ag/BSCF electrodes were comparatively studied using Fourier transform infrared spectra, environmental scanning electron microscopy, temperature-programmed oxygen desorption, X-ray diffraction, and electrochemical impedance spectroscopy. An area-specific resistance as low as 0.038 O cm2 was achieved for N2H4-reduced Ag/BSCF cathode at 600 °C. Carbonates were detected over the BSCF surface during the reduction of silver, which deteriorated both the charge-transfer process and diffusion process of HCHO-reduced Ag/BSCF cathode for the oxygen electrochemical reduction reaction. An anode-supported single cell with an N2H4-reduced Ag/BSCF cathode showed a peak power of 826 mW cm-2 at 600 °C. In comparison, only 672 mW cm-2 was observed with the HCHO-reduced Ag/BSCF cathode. © 2008 Elsevier B.V. All rights reserved. 2009 Journal Article http://hdl.handle.net/20.500.11937/39000 10.1016/j.jpowsour.2008.10.055 Elsevier SA restricted
spellingShingle Zhou, W.
Ran, R.
Cai, R.
Shao, Zongping
Jin, W.
Xu, N.
Effect of a reducing agent for silver on the electrochemical activity of an Ag/Ba0.5Sr0.5Co0.8Fe0.2O3-d electrode prepared by electroless deposition technique
title Effect of a reducing agent for silver on the electrochemical activity of an Ag/Ba0.5Sr0.5Co0.8Fe0.2O3-d electrode prepared by electroless deposition technique
title_full Effect of a reducing agent for silver on the electrochemical activity of an Ag/Ba0.5Sr0.5Co0.8Fe0.2O3-d electrode prepared by electroless deposition technique
title_fullStr Effect of a reducing agent for silver on the electrochemical activity of an Ag/Ba0.5Sr0.5Co0.8Fe0.2O3-d electrode prepared by electroless deposition technique
title_full_unstemmed Effect of a reducing agent for silver on the electrochemical activity of an Ag/Ba0.5Sr0.5Co0.8Fe0.2O3-d electrode prepared by electroless deposition technique
title_short Effect of a reducing agent for silver on the electrochemical activity of an Ag/Ba0.5Sr0.5Co0.8Fe0.2O3-d electrode prepared by electroless deposition technique
title_sort effect of a reducing agent for silver on the electrochemical activity of an ag/ba0.5sr0.5co0.8fe0.2o3-d electrode prepared by electroless deposition technique
url http://hdl.handle.net/20.500.11937/39000