Fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization

© 2015, Springer Science+Business Media New York. This paper presents the study on the growth of bundled titanium dioxide (TiO2) nanotubes via rapid breakdown anodization method by using chloride-based electrolyte. The effects of different ratios of deionized water (DI) to ethylene glycol (EG) on th...

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Main Authors: Cheong, Y., Yam, F., Ng, S., Hassan, Z., Low, It Meng
Format: Journal Article
Published: 2015
Online Access:http://hdl.handle.net/20.500.11937/37054
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author Cheong, Y.
Yam, F.
Ng, S.
Hassan, Z.
Ng, S.
Low, It Meng
author_facet Cheong, Y.
Yam, F.
Ng, S.
Hassan, Z.
Ng, S.
Low, It Meng
author_sort Cheong, Y.
building Curtin Institutional Repository
collection Online Access
description © 2015, Springer Science+Business Media New York. This paper presents the study on the growth of bundled titanium dioxide (TiO2) nanotubes via rapid breakdown anodization method by using chloride-based electrolyte. The effects of different ratios of deionized water (DI) to ethylene glycol (EG) on the morphological, structural and photoelectrochemical properties of the TiO2 nanotubes generated were investigated. Different ratios of DI:EG showed significant changes on the diameter of nanotube bundles. Besides that, X-ray diffraction measurements revealed that anatase phase of titanium dioxide appeared within the thermally treated samples. Scherrer method was applied to calculate the mean crystallite size of the crystal growth in this study. The photoelectrochemical properties of TiO2 nanotube bundles were characterized by using three-electrode photoelectrochemical cell and showed good photocurrent response and stability.
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institution Curtin University Malaysia
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spelling curtin-20.500.11937-370542017-09-13T15:24:46Z Fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization Cheong, Y. Yam, F. Ng, S. Hassan, Z. Ng, S. Low, It Meng © 2015, Springer Science+Business Media New York. This paper presents the study on the growth of bundled titanium dioxide (TiO2) nanotubes via rapid breakdown anodization method by using chloride-based electrolyte. The effects of different ratios of deionized water (DI) to ethylene glycol (EG) on the morphological, structural and photoelectrochemical properties of the TiO2 nanotubes generated were investigated. Different ratios of DI:EG showed significant changes on the diameter of nanotube bundles. Besides that, X-ray diffraction measurements revealed that anatase phase of titanium dioxide appeared within the thermally treated samples. Scherrer method was applied to calculate the mean crystallite size of the crystal growth in this study. The photoelectrochemical properties of TiO2 nanotube bundles were characterized by using three-electrode photoelectrochemical cell and showed good photocurrent response and stability. 2015 Journal Article http://hdl.handle.net/20.500.11937/37054 10.1007/s10934-015-0024-8 restricted
spellingShingle Cheong, Y.
Yam, F.
Ng, S.
Hassan, Z.
Ng, S.
Low, It Meng
Fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization
title Fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization
title_full Fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization
title_fullStr Fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization
title_full_unstemmed Fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization
title_short Fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization
title_sort fabrication of titanium dioxide nanotubes in fluoride-free electrolyte via rapid breakdown anodization
url http://hdl.handle.net/20.500.11937/37054