Activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol

Several activated carbons (ACs) were used as metal-free catalysts for degradation of a toxic organiccompound, phenol, in the presence of different oxidants, H2O2, peroxydisulfate (PS) and peroxymonosulfate (PMS). It was found that ACs were effective in heterogeneous activation of PMS toproduce sulfa...

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Main Authors: Saputra, Edy, Muhammad, Syaifullah, Sun, Hongqi, Wang, Shaobin
Format: Journal Article
Published: Royal Society of Chemistry 2013
Online Access:http://purl.org/au-research/grants/arc/DP130101319
http://hdl.handle.net/20.500.11937/36965
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author Saputra, Edy
Muhammad, Syaifullah
Sun, Hongqi
Wang, Shaobin
author_facet Saputra, Edy
Muhammad, Syaifullah
Sun, Hongqi
Wang, Shaobin
author_sort Saputra, Edy
building Curtin Institutional Repository
collection Online Access
description Several activated carbons (ACs) were used as metal-free catalysts for degradation of a toxic organiccompound, phenol, in the presence of different oxidants, H2O2, peroxydisulfate (PS) and peroxymonosulfate (PMS). It was found that ACs were effective in heterogeneous activation of PMS toproduce sulfate radicals for degradation of phenol, much better than H2O2 and PS. Particle size of AC significantly influenced AC activity, and powder AC was much more effective than granular AC. The complete phenol removal could be achieved in 15 min on powder activated carbon (PAC) under the conditions of [phenol] = 25 mg L-1, [PAC] = 0.2 g L-1, [PMS] = 6.5 mmol L-1, and T = 25 degrees Celcius. It was also found that phenol degradation was significantly influenced by PMS loading, catalyst loading, phenol concentration and temperature. Surface activation of PMS and phenol adsorption played important roles in phenol degradation. Surface coverage by intermediate adsorption and structural change induced deactivation of AC and catalytic activity could be partially recovered by regeneration using calcination.
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spelling curtin-20.500.11937-369652022-10-06T05:16:43Z Activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol Saputra, Edy Muhammad, Syaifullah Sun, Hongqi Wang, Shaobin Several activated carbons (ACs) were used as metal-free catalysts for degradation of a toxic organiccompound, phenol, in the presence of different oxidants, H2O2, peroxydisulfate (PS) and peroxymonosulfate (PMS). It was found that ACs were effective in heterogeneous activation of PMS toproduce sulfate radicals for degradation of phenol, much better than H2O2 and PS. Particle size of AC significantly influenced AC activity, and powder AC was much more effective than granular AC. The complete phenol removal could be achieved in 15 min on powder activated carbon (PAC) under the conditions of [phenol] = 25 mg L-1, [PAC] = 0.2 g L-1, [PMS] = 6.5 mmol L-1, and T = 25 degrees Celcius. It was also found that phenol degradation was significantly influenced by PMS loading, catalyst loading, phenol concentration and temperature. Surface activation of PMS and phenol adsorption played important roles in phenol degradation. Surface coverage by intermediate adsorption and structural change induced deactivation of AC and catalytic activity could be partially recovered by regeneration using calcination. 2013 Journal Article http://hdl.handle.net/20.500.11937/36965 10.1039/c3ra42455c http://purl.org/au-research/grants/arc/DP130101319 Royal Society of Chemistry fulltext
spellingShingle Saputra, Edy
Muhammad, Syaifullah
Sun, Hongqi
Wang, Shaobin
Activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol
title Activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol
title_full Activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol
title_fullStr Activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol
title_full_unstemmed Activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol
title_short Activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol
title_sort activated carbons as green and effective catalysts for generation of reactive radicals in degradation of aqueous phenol
url http://purl.org/au-research/grants/arc/DP130101319
http://hdl.handle.net/20.500.11937/36965