Synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process

Nano-sized La0.6Sr0.4Co0.2Fe 0.8O3-d (LSCF) and La0.8Sr 0.2MnO3-d (LSM) oxides were synthesized by a simple in situ sol-gel derived carbon templating process. Nano-sized LSCF-carbon and LSM-carbon composites were first obtained with a grain size of 20-30 nm. Further calcination of the obtained compo...

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Main Authors: Zhou, W., Ran, R., Shao, Zongping, Jin, W., Xu, N.
Format: Journal Article
Published: Indian Academy of Sciences 2010
Online Access:http://hdl.handle.net/20.500.11937/35263
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author Zhou, W.
Ran, R.
Shao, Zongping
Jin, W.
Xu, N.
author_facet Zhou, W.
Ran, R.
Shao, Zongping
Jin, W.
Xu, N.
author_sort Zhou, W.
building Curtin Institutional Repository
collection Online Access
description Nano-sized La0.6Sr0.4Co0.2Fe 0.8O3-d (LSCF) and La0.8Sr 0.2MnO3-d (LSM) oxides were synthesized by a simple in situ sol-gel derived carbon templating process. Nano-sized LSCF-carbon and LSM-carbon composites were first obtained with a grain size of 20-30 nm. Further calcination of the obtained composites under air resulted in the nano-sized pure-phase perovskites with crystalline size of as small as 14 nm. Such a decrease in crystalline size of perovskite via the indirect calcination process was ascribed to the suppressing effect of carbon in the grain growth of perovskite. Furthermore, when the in situ created carbon was applied as a template for pore forming, a highly porous perovskite sintering body packing from the nano-sized perovskite oxide was obtained. © Indian Academy of Sciences.
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institution Curtin University Malaysia
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publishDate 2010
publisher Indian Academy of Sciences
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spelling curtin-20.500.11937-352632017-12-11T04:21:53Z Synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process Zhou, W. Ran, R. Shao, Zongping Jin, W. Xu, N. Nano-sized La0.6Sr0.4Co0.2Fe 0.8O3-d (LSCF) and La0.8Sr 0.2MnO3-d (LSM) oxides were synthesized by a simple in situ sol-gel derived carbon templating process. Nano-sized LSCF-carbon and LSM-carbon composites were first obtained with a grain size of 20-30 nm. Further calcination of the obtained composites under air resulted in the nano-sized pure-phase perovskites with crystalline size of as small as 14 nm. Such a decrease in crystalline size of perovskite via the indirect calcination process was ascribed to the suppressing effect of carbon in the grain growth of perovskite. Furthermore, when the in situ created carbon was applied as a template for pore forming, a highly porous perovskite sintering body packing from the nano-sized perovskite oxide was obtained. © Indian Academy of Sciences. 2010 Journal Article http://hdl.handle.net/20.500.11937/35263 10.1007/s12034-010-0056-2 Indian Academy of Sciences restricted
spellingShingle Zhou, W.
Ran, R.
Shao, Zongping
Jin, W.
Xu, N.
Synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process
title Synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process
title_full Synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process
title_fullStr Synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process
title_full_unstemmed Synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process
title_short Synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process
title_sort synthesis of nano-particle and highly porous conducting perovskites from simple in situ sol-gel derived carbon templating process
url http://hdl.handle.net/20.500.11937/35263