Electrochemical investigation of gold uptake from chloride solution by magnetite

An electrochemical method (potential sweep method) was utilized to investigate the nature of the absorbed gold on magnetite and to determine the gold sorption mechanism. A magnetite electrode was prepared in the laboratory, made in contact with a gold chloride solution at different conditions, and w...

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Main Authors: Alorro, Richard, Hiroyoshi, N., Kijitani, H., Ito, M., Tsunekawa, M.
Format: Journal Article
Published: Taylor and Francis Inc. 2015
Online Access:http://hdl.handle.net/20.500.11937/34611
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author Alorro, Richard
Hiroyoshi, N.
Kijitani, H.
Ito, M.
Tsunekawa, M.
author_facet Alorro, Richard
Hiroyoshi, N.
Kijitani, H.
Ito, M.
Tsunekawa, M.
author_sort Alorro, Richard
building Curtin Institutional Repository
collection Online Access
description An electrochemical method (potential sweep method) was utilized to investigate the nature of the absorbed gold on magnetite and to determine the gold sorption mechanism. A magnetite electrode was prepared in the laboratory, made in contact with a gold chloride solution at different conditions, and was subjected to cyclic voltammetry. The cyclic voltammogram of the magnetite electrode pretreated in a gold chloride solution recorded an anodic current peak at around 1.0 V (vs. Ag/AgCl), which corresponds to the current generated for the anodic dissolution of metallic gold in a chloride medium. The results of the electrochemical experiments suggest that gold chloride complexes are reduced to metallic gold on the surface of magnetite. A four-stage gold uptake mechanism was proposed: (i) the transport of AuC14- from the bulk solution to the magnetite surface, (ii) adsorption of AuC14- ions on magnetite surface by electrostatic attraction, (iii) electrochemical reduction of AuC14- to metallic Au, and (iv) the transport of soluble species to the solution phase. The electrochemical investigation also revealed that Fe3+ ions released from magnetite into the solution, suppressed the gold uptake at the acidic pH region.
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institution Curtin University Malaysia
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spelling curtin-20.500.11937-346112017-09-13T15:10:44Z Electrochemical investigation of gold uptake from chloride solution by magnetite Alorro, Richard Hiroyoshi, N. Kijitani, H. Ito, M. Tsunekawa, M. An electrochemical method (potential sweep method) was utilized to investigate the nature of the absorbed gold on magnetite and to determine the gold sorption mechanism. A magnetite electrode was prepared in the laboratory, made in contact with a gold chloride solution at different conditions, and was subjected to cyclic voltammetry. The cyclic voltammogram of the magnetite electrode pretreated in a gold chloride solution recorded an anodic current peak at around 1.0 V (vs. Ag/AgCl), which corresponds to the current generated for the anodic dissolution of metallic gold in a chloride medium. The results of the electrochemical experiments suggest that gold chloride complexes are reduced to metallic gold on the surface of magnetite. A four-stage gold uptake mechanism was proposed: (i) the transport of AuC14- from the bulk solution to the magnetite surface, (ii) adsorption of AuC14- ions on magnetite surface by electrostatic attraction, (iii) electrochemical reduction of AuC14- to metallic Au, and (iv) the transport of soluble species to the solution phase. The electrochemical investigation also revealed that Fe3+ ions released from magnetite into the solution, suppressed the gold uptake at the acidic pH region. 2015 Journal Article http://hdl.handle.net/20.500.11937/34611 10.1080/08827508.2015.1004406 Taylor and Francis Inc. restricted
spellingShingle Alorro, Richard
Hiroyoshi, N.
Kijitani, H.
Ito, M.
Tsunekawa, M.
Electrochemical investigation of gold uptake from chloride solution by magnetite
title Electrochemical investigation of gold uptake from chloride solution by magnetite
title_full Electrochemical investigation of gold uptake from chloride solution by magnetite
title_fullStr Electrochemical investigation of gold uptake from chloride solution by magnetite
title_full_unstemmed Electrochemical investigation of gold uptake from chloride solution by magnetite
title_short Electrochemical investigation of gold uptake from chloride solution by magnetite
title_sort electrochemical investigation of gold uptake from chloride solution by magnetite
url http://hdl.handle.net/20.500.11937/34611