Radiolysis of acetic acid aqueous solutions—Effect of pH and persulfate addition

The degradation of acetic acid in aqueous solution by ionizing radiation was studied. The radiolysis of acetic acid solution induces the almost complete degradation and mineralization of this compound. The high yield of acetic acid mineralization is explained by the degradation of oxalic acid by sol...

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Main Authors: Criquet, Justine, Karpel Vel Leitner, N.
Format: Journal Article
Published: Elsevier BV 2011
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/32370
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author Criquet, Justine
Karpel Vel Leitner, N.
author_facet Criquet, Justine
Karpel Vel Leitner, N.
author_sort Criquet, Justine
building Curtin Institutional Repository
collection Online Access
description The degradation of acetic acid in aqueous solution by ionizing radiation was studied. The radiolysis of acetic acid solution induces the almost complete degradation and mineralization of this compound. The high yield of acetic acid mineralization is explained by the degradation of oxalic acid by solvated electron. The degradation of acetic acid depends on the pH of the solution. The best degradation is observed at pH 4.5 due to the higher rate constant of reaction of acetate with hydroxyl radicals and the competitive reactions of inorganic carbon which occur at higher pH. The influence of persulfate ion (S2O82−) addition that forms the sulfate radical (SO4 −) during irradiation in solution was examined. The persulfate addition induces an almost constant degradation of acetic acid whatever the initial pH of the solution. The decrease of pH during the persulfate radiolysis partly explains the high degradation observed. But the additional radicals formed by the persulfate introduction also improve the degradation.
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institution Curtin University Malaysia
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publishDate 2011
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spelling curtin-20.500.11937-323702017-09-13T16:08:11Z Radiolysis of acetic acid aqueous solutions—Effect of pH and persulfate addition Criquet, Justine Karpel Vel Leitner, N. Water treatment Oxidation Sulfate radical Carboxylic acid e-Beam The degradation of acetic acid in aqueous solution by ionizing radiation was studied. The radiolysis of acetic acid solution induces the almost complete degradation and mineralization of this compound. The high yield of acetic acid mineralization is explained by the degradation of oxalic acid by solvated electron. The degradation of acetic acid depends on the pH of the solution. The best degradation is observed at pH 4.5 due to the higher rate constant of reaction of acetate with hydroxyl radicals and the competitive reactions of inorganic carbon which occur at higher pH. The influence of persulfate ion (S2O82−) addition that forms the sulfate radical (SO4 −) during irradiation in solution was examined. The persulfate addition induces an almost constant degradation of acetic acid whatever the initial pH of the solution. The decrease of pH during the persulfate radiolysis partly explains the high degradation observed. But the additional radicals formed by the persulfate introduction also improve the degradation. 2011 Journal Article http://hdl.handle.net/20.500.11937/32370 10.1016/j.cej.2011.07.079 Elsevier BV restricted
spellingShingle Water treatment
Oxidation
Sulfate radical
Carboxylic acid
e-Beam
Criquet, Justine
Karpel Vel Leitner, N.
Radiolysis of acetic acid aqueous solutions—Effect of pH and persulfate addition
title Radiolysis of acetic acid aqueous solutions—Effect of pH and persulfate addition
title_full Radiolysis of acetic acid aqueous solutions—Effect of pH and persulfate addition
title_fullStr Radiolysis of acetic acid aqueous solutions—Effect of pH and persulfate addition
title_full_unstemmed Radiolysis of acetic acid aqueous solutions—Effect of pH and persulfate addition
title_short Radiolysis of acetic acid aqueous solutions—Effect of pH and persulfate addition
title_sort radiolysis of acetic acid aqueous solutions—effect of ph and persulfate addition
topic Water treatment
Oxidation
Sulfate radical
Carboxylic acid
e-Beam
url http://hdl.handle.net/20.500.11937/32370