In situ high pressure NMR study of the direct synthesis of NaAlH 4

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In situ high pressure NMR study of the direct synthesis of NaAlH 4

The direct synthesis of NaAlH4 has been studied, for the first time, by in situ27Al and 23Na wide-line NMR spectroscopy using high pressure NMR apparatus. Na3AlH6 formation is observed within two minutes of hydrogen addition, while NaAlH4 is detected after a total of four minutes. This indicates the...

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Bibliographic Details
Main Authors:	Humphries, Terry, Birkmire, D., Hauback, B., Sean McGrady, G., Jensen, C.
Format:	Journal Article
Published:	2013
Online Access:	http://hdl.handle.net/20.500.11937/27922

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