Influence of crystal structure on the electrochemical performance of A-site-deficient Sr1-sNb0.1Co0.9O3-dperovskite cathodes

The creation of A-site cation defects within a perovskite oxide can substantially alter the structure and properties of its stoichiometric analogue. In this work, we demonstrate that by vacating 2 and 5% of A-site cations from SrNb0.1Co0.9O3−δ (SNC1.00) perovskites (Sr1−sNb0.1Co0.9O3−δ, s = 0.02 and...

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Main Authors: Zhu, Y., Lin, Y., Shen, X., Sunarso, J., Zhou, W., Jiang, S., Su, D., Chen, F., Shao, Zongping
Format: Journal Article
Published: Royal Society of Chemistry 2014
Online Access:http://hdl.handle.net/20.500.11937/27773
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author Zhu, Y.
Lin, Y.
Shen, X.
Sunarso, J.
Zhou, W.
Jiang, S.
Su, D.
Chen, F.
Shao, Zongping
author_facet Zhu, Y.
Lin, Y.
Shen, X.
Sunarso, J.
Zhou, W.
Jiang, S.
Su, D.
Chen, F.
Shao, Zongping
author_sort Zhu, Y.
building Curtin Institutional Repository
collection Online Access
description The creation of A-site cation defects within a perovskite oxide can substantially alter the structure and properties of its stoichiometric analogue. In this work, we demonstrate that by vacating 2 and 5% of A-site cations from SrNb0.1Co0.9O3−δ (SNC1.00) perovskites (Sr1−sNb0.1Co0.9O3−δ, s = 0.02 and 0.05; denoted as SNC0.98 and SNC0.95, respectively), a Jahn–Teller (JT) distortion with varying extents takes place, leading to the formation of a modified crystal lattice within a the perovskite framework. Electrical conductivity, electrochemical performance, chemical compatibility and microstructure of Sr1−sNb0.1Co0.9O3−δ as cathodes for solid oxide fuel cells were evaluated. Among SNC1.00, SNC0.98 and SNC0.95, SNC0.95 (P4/mmm symmetry (#123)) which exhibits a large JT distortion in conjunction with charge-ordering of cobalt (Co) shows the best oxygen reduction reaction (ORR) activity at low temperature while SNC0.98 (P4mm symmetry (#99)), which displays a local JT distortion, shows the poorest performance.
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spelling curtin-20.500.11937-277732017-09-13T15:11:56Z Influence of crystal structure on the electrochemical performance of A-site-deficient Sr1-sNb0.1Co0.9O3-dperovskite cathodes Zhu, Y. Lin, Y. Shen, X. Sunarso, J. Zhou, W. Jiang, S. Su, D. Chen, F. Shao, Zongping The creation of A-site cation defects within a perovskite oxide can substantially alter the structure and properties of its stoichiometric analogue. In this work, we demonstrate that by vacating 2 and 5% of A-site cations from SrNb0.1Co0.9O3−δ (SNC1.00) perovskites (Sr1−sNb0.1Co0.9O3−δ, s = 0.02 and 0.05; denoted as SNC0.98 and SNC0.95, respectively), a Jahn–Teller (JT) distortion with varying extents takes place, leading to the formation of a modified crystal lattice within a the perovskite framework. Electrical conductivity, electrochemical performance, chemical compatibility and microstructure of Sr1−sNb0.1Co0.9O3−δ as cathodes for solid oxide fuel cells were evaluated. Among SNC1.00, SNC0.98 and SNC0.95, SNC0.95 (P4/mmm symmetry (#123)) which exhibits a large JT distortion in conjunction with charge-ordering of cobalt (Co) shows the best oxygen reduction reaction (ORR) activity at low temperature while SNC0.98 (P4mm symmetry (#99)), which displays a local JT distortion, shows the poorest performance. 2014 Journal Article http://hdl.handle.net/20.500.11937/27773 10.1039/c4ra06191h Royal Society of Chemistry restricted
spellingShingle Zhu, Y.
Lin, Y.
Shen, X.
Sunarso, J.
Zhou, W.
Jiang, S.
Su, D.
Chen, F.
Shao, Zongping
Influence of crystal structure on the electrochemical performance of A-site-deficient Sr1-sNb0.1Co0.9O3-dperovskite cathodes
title Influence of crystal structure on the electrochemical performance of A-site-deficient Sr1-sNb0.1Co0.9O3-dperovskite cathodes
title_full Influence of crystal structure on the electrochemical performance of A-site-deficient Sr1-sNb0.1Co0.9O3-dperovskite cathodes
title_fullStr Influence of crystal structure on the electrochemical performance of A-site-deficient Sr1-sNb0.1Co0.9O3-dperovskite cathodes
title_full_unstemmed Influence of crystal structure on the electrochemical performance of A-site-deficient Sr1-sNb0.1Co0.9O3-dperovskite cathodes
title_short Influence of crystal structure on the electrochemical performance of A-site-deficient Sr1-sNb0.1Co0.9O3-dperovskite cathodes
title_sort influence of crystal structure on the electrochemical performance of a-site-deficient sr1-snb0.1co0.9o3-dperovskite cathodes
url http://hdl.handle.net/20.500.11937/27773