Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode

A novel non enzymatic glucose sensor was developed based on the renewable Ni nanoparticle-loaded carbon nanofiber paste (NiCFP) electrode. The NiCF nano composite was prepared by combination of electro spinning technique with thermal treatment method. The scanning electron microscopy (SEM) and trans...

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Main Authors: Liu, Yang, Teng, H., Hou, H., You, T.
Format: Journal Article
Published: Elsevier BV 2009
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/27142
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author Liu, Yang
Teng, H.
Hou, H.
You, T.
author_facet Liu, Yang
Teng, H.
Hou, H.
You, T.
author_sort Liu, Yang
building Curtin Institutional Repository
collection Online Access
description A novel non enzymatic glucose sensor was developed based on the renewable Ni nanoparticle-loaded carbon nanofiber paste (NiCFP) electrode. The NiCF nano composite was prepared by combination of electro spinning technique with thermal treatment method. The scanning electron microscopy (SEM) and transmission electron microscopy (TEM) images showed that large amounts of spherical nanoparticles were well dispersed on the surface or embedded in the carbon nanofibers. And the nanoparticles were composed of Ni and NiO, as revealed by energy dispersive X-ray spectroscopy (EDX) and X-ray powder diffraction (XRD). In application to nonenzymatic glucose determination, the renewable NiCFP electrodes, which were constructed by simply mixing the electrospun nano composite with mineral oil, exhibited strong and fast amperometric response without being poisoned by chloride ions. Low detection limit of 1M with wide linear range from 2M to 2.5mM (R = 0.9997) could be obtained. The current response of the proposed glucose sensor was highly sensitive and stable, attributing to the electro catalytic performance of the firmly embedded Ni nanoparticles as well as the chemical inertness of the carbon-based electrode. The good analytical performance, low cost and straightforward preparation method made this novel electrode material promising for the development of effective glucose sensor.
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institution Curtin University Malaysia
institution_category Local University
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publishDate 2009
publisher Elsevier BV
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spelling curtin-20.500.11937-271422017-09-13T15:30:51Z Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode Liu, Yang Teng, H. Hou, H. You, T. Electrospinning Ni nanoparticle-loaded carbon nanofiber Glucose Renewable electrode Nonenzymatic sensor A novel non enzymatic glucose sensor was developed based on the renewable Ni nanoparticle-loaded carbon nanofiber paste (NiCFP) electrode. The NiCF nano composite was prepared by combination of electro spinning technique with thermal treatment method. The scanning electron microscopy (SEM) and transmission electron microscopy (TEM) images showed that large amounts of spherical nanoparticles were well dispersed on the surface or embedded in the carbon nanofibers. And the nanoparticles were composed of Ni and NiO, as revealed by energy dispersive X-ray spectroscopy (EDX) and X-ray powder diffraction (XRD). In application to nonenzymatic glucose determination, the renewable NiCFP electrodes, which were constructed by simply mixing the electrospun nano composite with mineral oil, exhibited strong and fast amperometric response without being poisoned by chloride ions. Low detection limit of 1M with wide linear range from 2M to 2.5mM (R = 0.9997) could be obtained. The current response of the proposed glucose sensor was highly sensitive and stable, attributing to the electro catalytic performance of the firmly embedded Ni nanoparticles as well as the chemical inertness of the carbon-based electrode. The good analytical performance, low cost and straightforward preparation method made this novel electrode material promising for the development of effective glucose sensor. 2009 Journal Article http://hdl.handle.net/20.500.11937/27142 10.1016/j.bios.2009.04.032 Elsevier BV restricted
spellingShingle Electrospinning
Ni nanoparticle-loaded carbon nanofiber
Glucose
Renewable electrode
Nonenzymatic sensor
Liu, Yang
Teng, H.
Hou, H.
You, T.
Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode
title Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode
title_full Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode
title_fullStr Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode
title_full_unstemmed Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode
title_short Nonenzymatic glucose sensor based on renewable electrospun Ni nanoparticle-loaded carbon nanofiber paste electrode
title_sort nonenzymatic glucose sensor based on renewable electrospun ni nanoparticle-loaded carbon nanofiber paste electrode
topic Electrospinning
Ni nanoparticle-loaded carbon nanofiber
Glucose
Renewable electrode
Nonenzymatic sensor
url http://hdl.handle.net/20.500.11937/27142