Leaching Characteristics of Organic and Inorganic Matter from Biomass by Water: Differences between Batch and Semi-continuous Operations

Over 30% and ~2% (on a carbon basis) organic matter can be leached from mallee leaf and wood by water, respectively, producing acidic leachates containing organic acids. As a result, there are significant differences in the leaching characteristics of both organic and inorganic species in biomass be...

Full description

Bibliographic Details
Main Authors: Liaw, Sui Boon, Wu, Hongwei
Format: Journal Article
Published: American Chemical Society 2013
Online Access:http://hdl.handle.net/20.500.11937/25735
_version_ 1848751790472822784
author Liaw, Sui Boon
Wu, Hongwei
author_facet Liaw, Sui Boon
Wu, Hongwei
author_sort Liaw, Sui Boon
building Curtin Institutional Repository
collection Online Access
description Over 30% and ~2% (on a carbon basis) organic matter can be leached from mallee leaf and wood by water, respectively, producing acidic leachates containing organic acids. As a result, there are significant differences in the leaching characteristics of both organic and inorganic species in biomass between batch and semi-continuous leaching operations. Under conventional batch leaching, the acidic leachate continuously contacts the biomass for a prolonged period, resulting in the leaching of at least some water-insoluble inorganic species (e.g., organically bound) from biomass. Therefore, the batch leaching method clearly overestimates the amount of water-soluble inorganic species in biomass and exhibits two-step leaching kinetics, i.e. a rapid leaching step for an initial short period followed by a slow leaching step for a relatively long period. This study further develops a semi-continuous leaching method to address this issue via minimizing the contact between the leachate and the biomass sample. The semi-continuous leaching quantifies the true water-soluble inorganic species in biomass. Its leaching kinetics include only the first rapid leaching step, with the disappearance of the second slow-leaching step due to the absence of the interaction between acidic leachate and biomass.The results suggest that in the sequential extraction scheme used in chemical fractionation, semi-continuous (instead of batch) water leaching method should be used for quantifying water-soluble inorganic species in biomass. Attention should also be paid to the potentially substantial loss of fuel materials when utilizing water leaching as a pretreatment method to remove inherent inorganic species in biomass for fuel quality improvement. As result of overestimating water-soluble inorganic species and loss of organic matter, care must be taken when using water batch washing as a method for studying the effect of the inherent water-soluble inorganic species on thermochemical reactions of biomass.
first_indexed 2025-11-14T07:58:19Z
format Journal Article
id curtin-20.500.11937-25735
institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T07:58:19Z
publishDate 2013
publisher American Chemical Society
recordtype eprints
repository_type Digital Repository
spelling curtin-20.500.11937-257352017-09-13T15:16:05Z Leaching Characteristics of Organic and Inorganic Matter from Biomass by Water: Differences between Batch and Semi-continuous Operations Liaw, Sui Boon Wu, Hongwei Over 30% and ~2% (on a carbon basis) organic matter can be leached from mallee leaf and wood by water, respectively, producing acidic leachates containing organic acids. As a result, there are significant differences in the leaching characteristics of both organic and inorganic species in biomass between batch and semi-continuous leaching operations. Under conventional batch leaching, the acidic leachate continuously contacts the biomass for a prolonged period, resulting in the leaching of at least some water-insoluble inorganic species (e.g., organically bound) from biomass. Therefore, the batch leaching method clearly overestimates the amount of water-soluble inorganic species in biomass and exhibits two-step leaching kinetics, i.e. a rapid leaching step for an initial short period followed by a slow leaching step for a relatively long period. This study further develops a semi-continuous leaching method to address this issue via minimizing the contact between the leachate and the biomass sample. The semi-continuous leaching quantifies the true water-soluble inorganic species in biomass. Its leaching kinetics include only the first rapid leaching step, with the disappearance of the second slow-leaching step due to the absence of the interaction between acidic leachate and biomass.The results suggest that in the sequential extraction scheme used in chemical fractionation, semi-continuous (instead of batch) water leaching method should be used for quantifying water-soluble inorganic species in biomass. Attention should also be paid to the potentially substantial loss of fuel materials when utilizing water leaching as a pretreatment method to remove inherent inorganic species in biomass for fuel quality improvement. As result of overestimating water-soluble inorganic species and loss of organic matter, care must be taken when using water batch washing as a method for studying the effect of the inherent water-soluble inorganic species on thermochemical reactions of biomass. 2013 Journal Article http://hdl.handle.net/20.500.11937/25735 10.1021/ie3031168 American Chemical Society restricted
spellingShingle Liaw, Sui Boon
Wu, Hongwei
Leaching Characteristics of Organic and Inorganic Matter from Biomass by Water: Differences between Batch and Semi-continuous Operations
title Leaching Characteristics of Organic and Inorganic Matter from Biomass by Water: Differences between Batch and Semi-continuous Operations
title_full Leaching Characteristics of Organic and Inorganic Matter from Biomass by Water: Differences between Batch and Semi-continuous Operations
title_fullStr Leaching Characteristics of Organic and Inorganic Matter from Biomass by Water: Differences between Batch and Semi-continuous Operations
title_full_unstemmed Leaching Characteristics of Organic and Inorganic Matter from Biomass by Water: Differences between Batch and Semi-continuous Operations
title_short Leaching Characteristics of Organic and Inorganic Matter from Biomass by Water: Differences between Batch and Semi-continuous Operations
title_sort leaching characteristics of organic and inorganic matter from biomass by water: differences between batch and semi-continuous operations
url http://hdl.handle.net/20.500.11937/25735