Transformation of chlorine in NaCl-loaded Victorian brown coal during the gasification in steam

This study is to examine the changes in Cl volatilizations and chemical forms in NaCl-loaded Victorian brown coal during gasification in steam at 800°C using Cl K-edge X-ray absorption near-edge structure (XANES) spectroscopy. The char samples were prepared in a novel one-stage fluidised-bed/fixed-b...

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Main Authors: Zhang, Shu, Asadullah, M., Hocking, R., Lin, J., Li, Chun-Zhu
Format: Journal Article
Published: 2012
Online Access:http://hdl.handle.net/20.500.11937/24098
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author Zhang, Shu
Asadullah, M.
Hocking, R.
Lin, J.
Li, Chun-Zhu
author_facet Zhang, Shu
Asadullah, M.
Hocking, R.
Lin, J.
Li, Chun-Zhu
author_sort Zhang, Shu
building Curtin Institutional Repository
collection Online Access
description This study is to examine the changes in Cl volatilizations and chemical forms in NaCl-loaded Victorian brown coal during gasification in steam at 800°C using Cl K-edge X-ray absorption near-edge structure (XANES) spectroscopy. The char samples were prepared in a novel one-stage fluidised-bed/fixed-bed quartz reactor at a fast heating rate. The samples were then collected and sealed in an argon-filled bag in order to minimise possible oxidation of char and Cl by air prior to analysis by XANES. Char-steam reactions were found to significantly affect the transformation of Cl, including the possible formation of chlorine-containing organic structures. On the other hand, volatile-char interactions during the gasification appeared to enhance the Cl retention and prevent the formation of organic chlorine compounds in chars.
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institution Curtin University Malaysia
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last_indexed 2025-11-14T07:51:05Z
publishDate 2012
recordtype eprints
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spelling curtin-20.500.11937-240982017-09-13T13:56:21Z Transformation of chlorine in NaCl-loaded Victorian brown coal during the gasification in steam Zhang, Shu Asadullah, M. Hocking, R. Lin, J. Li, Chun-Zhu This study is to examine the changes in Cl volatilizations and chemical forms in NaCl-loaded Victorian brown coal during gasification in steam at 800°C using Cl K-edge X-ray absorption near-edge structure (XANES) spectroscopy. The char samples were prepared in a novel one-stage fluidised-bed/fixed-bed quartz reactor at a fast heating rate. The samples were then collected and sealed in an argon-filled bag in order to minimise possible oxidation of char and Cl by air prior to analysis by XANES. Char-steam reactions were found to significantly affect the transformation of Cl, including the possible formation of chlorine-containing organic structures. On the other hand, volatile-char interactions during the gasification appeared to enhance the Cl retention and prevent the formation of organic chlorine compounds in chars. 2012 Journal Article http://hdl.handle.net/20.500.11937/24098 10.1016/S1872-5813(13)60005-5 restricted
spellingShingle Zhang, Shu
Asadullah, M.
Hocking, R.
Lin, J.
Li, Chun-Zhu
Transformation of chlorine in NaCl-loaded Victorian brown coal during the gasification in steam
title Transformation of chlorine in NaCl-loaded Victorian brown coal during the gasification in steam
title_full Transformation of chlorine in NaCl-loaded Victorian brown coal during the gasification in steam
title_fullStr Transformation of chlorine in NaCl-loaded Victorian brown coal during the gasification in steam
title_full_unstemmed Transformation of chlorine in NaCl-loaded Victorian brown coal during the gasification in steam
title_short Transformation of chlorine in NaCl-loaded Victorian brown coal during the gasification in steam
title_sort transformation of chlorine in nacl-loaded victorian brown coal during the gasification in steam
url http://hdl.handle.net/20.500.11937/24098