Growth and optical spectroscopy of KPb2Cl5 crystal containing Mn2+

KPb2Cl5:Mn2+ crystal with sizes of centimeters has been successfully grown by a modified Bridgman method. The electronic spectra of Mn2+ in the title compound have been measured at different temperatures and compared, revealing that the red emission observed at 10 and 77 K in the spectral range from...

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Main Authors: Jia, Guohua, Wang, H., Wang, C., Zhao, S., Deng, D., Huang, L., Hua, Y., Li, C., Xu, S.
Format: Journal Article
Published: Elsevier B.V. 2011
Online Access:http://hdl.handle.net/20.500.11937/22735
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author Jia, Guohua
Wang, H.
Wang, C.
Zhao, S.
Deng, D.
Huang, L.
Hua, Y.
Li, C.
Xu, S.
author_facet Jia, Guohua
Wang, H.
Wang, C.
Zhao, S.
Deng, D.
Huang, L.
Hua, Y.
Li, C.
Xu, S.
author_sort Jia, Guohua
building Curtin Institutional Repository
collection Online Access
description KPb2Cl5:Mn2+ crystal with sizes of centimeters has been successfully grown by a modified Bridgman method. The electronic spectra of Mn2+ in the title compound have been measured at different temperatures and compared, revealing that the red emission observed at 10 and 77 K in the spectral range from 500 to 800 nm, which vanishes at room temperature, is associated with the radiation from Pb2+ ions with adjacent defects whereas the orange-red emission in the spectral range from 530 to 680 nm can be undoubtedly attributed to the spin forbidden transition 4T1g (4G) ? 6A 1g(6S) of Mn2+. The electronic excitation spectra are interpreted in a strong crystal field scheme with the use of the Tanabe-Sugano diagram. Good agreement with the experimental spectroscopic data is obtained with the use of crystal field splitting parameter 10Dq = 7902 cm-1, Racah parameters B = 618 cm-1, and C = 3549 cm -1. © 2011 Elsevier B.V. All rights reserved.
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format Journal Article
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institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T07:45:01Z
publishDate 2011
publisher Elsevier B.V.
recordtype eprints
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spelling curtin-20.500.11937-227352023-08-02T06:39:07Z Growth and optical spectroscopy of KPb2Cl5 crystal containing Mn2+ Jia, Guohua Wang, H. Wang, C. Zhao, S. Deng, D. Huang, L. Hua, Y. Li, C. Xu, S. KPb2Cl5:Mn2+ crystal with sizes of centimeters has been successfully grown by a modified Bridgman method. The electronic spectra of Mn2+ in the title compound have been measured at different temperatures and compared, revealing that the red emission observed at 10 and 77 K in the spectral range from 500 to 800 nm, which vanishes at room temperature, is associated with the radiation from Pb2+ ions with adjacent defects whereas the orange-red emission in the spectral range from 530 to 680 nm can be undoubtedly attributed to the spin forbidden transition 4T1g (4G) ? 6A 1g(6S) of Mn2+. The electronic excitation spectra are interpreted in a strong crystal field scheme with the use of the Tanabe-Sugano diagram. Good agreement with the experimental spectroscopic data is obtained with the use of crystal field splitting parameter 10Dq = 7902 cm-1, Racah parameters B = 618 cm-1, and C = 3549 cm -1. © 2011 Elsevier B.V. All rights reserved. 2011 Journal Article http://hdl.handle.net/20.500.11937/22735 10.1016/j.jallcom.2011.05.010 Elsevier B.V. restricted
spellingShingle Jia, Guohua
Wang, H.
Wang, C.
Zhao, S.
Deng, D.
Huang, L.
Hua, Y.
Li, C.
Xu, S.
Growth and optical spectroscopy of KPb2Cl5 crystal containing Mn2+
title Growth and optical spectroscopy of KPb2Cl5 crystal containing Mn2+
title_full Growth and optical spectroscopy of KPb2Cl5 crystal containing Mn2+
title_fullStr Growth and optical spectroscopy of KPb2Cl5 crystal containing Mn2+
title_full_unstemmed Growth and optical spectroscopy of KPb2Cl5 crystal containing Mn2+
title_short Growth and optical spectroscopy of KPb2Cl5 crystal containing Mn2+
title_sort growth and optical spectroscopy of kpb2cl5 crystal containing mn2+
url http://hdl.handle.net/20.500.11937/22735