NiO reduction with hydrogen and light hydrocarbons: Contrast between SiO2-supported and unsupported NiO nanoparticles

The reduction of solid metal oxide by hydrogen or hydrocarbon gases represents a class of reactions that are important to various technological applications. This study investigates the reduction of unsupported NiO nanoparticles and silica-supported NiO with different reducing gases (hydrogen, metha...

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Main Authors: Syed-Hassan, Syed, Li, Chun-Zhu
Format: Journal Article
Published: Elsevier B.V. 2011
Online Access:http://hdl.handle.net/20.500.11937/21930
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author Syed-Hassan, Syed
Li, Chun-Zhu
author_facet Syed-Hassan, Syed
Li, Chun-Zhu
author_sort Syed-Hassan, Syed
building Curtin Institutional Repository
collection Online Access
description The reduction of solid metal oxide by hydrogen or hydrocarbon gases represents a class of reactions that are important to various technological applications. This study investigates the reduction of unsupported NiO nanoparticles and silica-supported NiO with different reducing gases (hydrogen, methane and ethane) in the temperature range of 500–600 °C. It was found that, in addition to the reaction and mass transfer of molecular species, the fates and activities of surface-formed radical species have to be considered in explaining the kinetics of nickel oxide reduction. It is believed that the desorption of hydrocarbon radicals from the particle surface has significantly slowed down the reduction of unsupported NiO nanoparticles. The ease with which a radical migrates from its generation site on a metallic island to the Ni–NiO surface boundary, on the other hand, is an important rate-determining factor in the reduction of silica-supported NiO.
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spelling curtin-20.500.11937-219302017-09-13T13:54:25Z NiO reduction with hydrogen and light hydrocarbons: Contrast between SiO2-supported and unsupported NiO nanoparticles Syed-Hassan, Syed Li, Chun-Zhu The reduction of solid metal oxide by hydrogen or hydrocarbon gases represents a class of reactions that are important to various technological applications. This study investigates the reduction of unsupported NiO nanoparticles and silica-supported NiO with different reducing gases (hydrogen, methane and ethane) in the temperature range of 500–600 °C. It was found that, in addition to the reaction and mass transfer of molecular species, the fates and activities of surface-formed radical species have to be considered in explaining the kinetics of nickel oxide reduction. It is believed that the desorption of hydrocarbon radicals from the particle surface has significantly slowed down the reduction of unsupported NiO nanoparticles. The ease with which a radical migrates from its generation site on a metallic island to the Ni–NiO surface boundary, on the other hand, is an important rate-determining factor in the reduction of silica-supported NiO. 2011 Journal Article http://hdl.handle.net/20.500.11937/21930 10.1016/j.apcata.2011.03.033 Elsevier B.V. restricted
spellingShingle Syed-Hassan, Syed
Li, Chun-Zhu
NiO reduction with hydrogen and light hydrocarbons: Contrast between SiO2-supported and unsupported NiO nanoparticles
title NiO reduction with hydrogen and light hydrocarbons: Contrast between SiO2-supported and unsupported NiO nanoparticles
title_full NiO reduction with hydrogen and light hydrocarbons: Contrast between SiO2-supported and unsupported NiO nanoparticles
title_fullStr NiO reduction with hydrogen and light hydrocarbons: Contrast between SiO2-supported and unsupported NiO nanoparticles
title_full_unstemmed NiO reduction with hydrogen and light hydrocarbons: Contrast between SiO2-supported and unsupported NiO nanoparticles
title_short NiO reduction with hydrogen and light hydrocarbons: Contrast between SiO2-supported and unsupported NiO nanoparticles
title_sort nio reduction with hydrogen and light hydrocarbons: contrast between sio2-supported and unsupported nio nanoparticles
url http://hdl.handle.net/20.500.11937/21930