Effect of Alkali and Alkaline Earth Metal Chlorides on Cellobiose Decomposition in Hot-Compressed Water

This paper reports a systematic study on the catalytic effect of alkali and alkaline earth metal (AAEM) chlorides on cellobiose decomposition in hot-compressed water (HCW) at 200–275 °C. The AAEM chlorides catalyze the cellobiose decomposition in HCW in the order of MgCl2 > CaCl2 > KCl > Na...

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Main Authors: Yu, Yun, Mohd Shafie, Zainun, Wu, Hongwei
Format: Journal Article
Published: American Chemical Society 2015
Online Access:http://hdl.handle.net/20.500.11937/21827
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author Yu, Yun
Mohd Shafie, Zainun
Wu, Hongwei
author_facet Yu, Yun
Mohd Shafie, Zainun
Wu, Hongwei
author_sort Yu, Yun
building Curtin Institutional Repository
collection Online Access
description This paper reports a systematic study on the catalytic effect of alkali and alkaline earth metal (AAEM) chlorides on cellobiose decomposition in hot-compressed water (HCW) at 200–275 °C. The AAEM chlorides catalyze the cellobiose decomposition in HCW in the order of MgCl2 > CaCl2 > KCl > NaCl. The presence of AAEM chlorides not only increases the reaction rate but also alters the selectivities of primary reactions of cellobiose decomposition. The isomerization reactions to cellobiulose and glucosyl-mannose are strongly promoted by these cations due to their interactions with cellobiose. The hydrolysis reaction to glucose is also promoted as the hydrolysis of hydrated metal complexes generates H3O+. However, the promotion effect on hydrolysis reaction is much weaker, resulting in reduced glucose selectivity in AAEM chloride solutions. Depending on the AAEM species, the secondary decomposition reactions of those primary products are selectively catalyzed in AAEM chloride solutions, thus greatly influencing the product distribution of cellobiose decomposition in HCW.
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institution Curtin University Malaysia
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spelling curtin-20.500.11937-218272017-09-13T13:55:05Z Effect of Alkali and Alkaline Earth Metal Chlorides on Cellobiose Decomposition in Hot-Compressed Water Yu, Yun Mohd Shafie, Zainun Wu, Hongwei This paper reports a systematic study on the catalytic effect of alkali and alkaline earth metal (AAEM) chlorides on cellobiose decomposition in hot-compressed water (HCW) at 200–275 °C. The AAEM chlorides catalyze the cellobiose decomposition in HCW in the order of MgCl2 > CaCl2 > KCl > NaCl. The presence of AAEM chlorides not only increases the reaction rate but also alters the selectivities of primary reactions of cellobiose decomposition. The isomerization reactions to cellobiulose and glucosyl-mannose are strongly promoted by these cations due to their interactions with cellobiose. The hydrolysis reaction to glucose is also promoted as the hydrolysis of hydrated metal complexes generates H3O+. However, the promotion effect on hydrolysis reaction is much weaker, resulting in reduced glucose selectivity in AAEM chloride solutions. Depending on the AAEM species, the secondary decomposition reactions of those primary products are selectively catalyzed in AAEM chloride solutions, thus greatly influencing the product distribution of cellobiose decomposition in HCW. 2015 Journal Article http://hdl.handle.net/20.500.11937/21827 10.1021/acs.iecr.5b01007 American Chemical Society restricted
spellingShingle Yu, Yun
Mohd Shafie, Zainun
Wu, Hongwei
Effect of Alkali and Alkaline Earth Metal Chlorides on Cellobiose Decomposition in Hot-Compressed Water
title Effect of Alkali and Alkaline Earth Metal Chlorides on Cellobiose Decomposition in Hot-Compressed Water
title_full Effect of Alkali and Alkaline Earth Metal Chlorides on Cellobiose Decomposition in Hot-Compressed Water
title_fullStr Effect of Alkali and Alkaline Earth Metal Chlorides on Cellobiose Decomposition in Hot-Compressed Water
title_full_unstemmed Effect of Alkali and Alkaline Earth Metal Chlorides on Cellobiose Decomposition in Hot-Compressed Water
title_short Effect of Alkali and Alkaline Earth Metal Chlorides on Cellobiose Decomposition in Hot-Compressed Water
title_sort effect of alkali and alkaline earth metal chlorides on cellobiose decomposition in hot-compressed water
url http://hdl.handle.net/20.500.11937/21827