Processes of oxidation and HCl-leaching of Tellnes ilmenite

Tellnes ilmenite is an important feedstock for the production of high-grade titanium pigment. The present study investigated the oxidation of ilmenite from Tellnes, Norway, at 700 °C in air and compared the leaching ability of pre-heated and non-heated Tellnes ilmenite in 20% HCl solution at 160 °C....

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Main Authors: Janssen, A., Putnis, Andrew
Format: Journal Article
Published: 2011
Online Access:http://hdl.handle.net/20.500.11937/21093
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author Janssen, A.
Putnis, Andrew
author_facet Janssen, A.
Putnis, Andrew
author_sort Janssen, A.
building Curtin Institutional Repository
collection Online Access
description Tellnes ilmenite is an important feedstock for the production of high-grade titanium pigment. The present study investigated the oxidation of ilmenite from Tellnes, Norway, at 700 °C in air and compared the leaching ability of pre-heated and non-heated Tellnes ilmenite in 20% HCl solution at 160 °C. Through the heat treatment, ilmenite (FeTiO3) is oxidized to hematite (Fe2O3) and rutile (TiO2) via a solid-state reaction mechanism. The leaching experiments revealed that after the pre-heating step the iron dissolution in the leaching process is limited due to the lower solubility of ferric iron in the hydrochloric acid. Furthermore, in both experiments the impurity phases such feldspar and orthopyroxene are less soluble in the hydrochloric acid and pollute the replacement product rutile because Si released from the impurity phases is incorporated in the rutile. The leaching reaction mechanism is interpreted as a pseudomorphic, interface-coupled dissolution-reprecipitation process, through which the external form of the parent ilmenite as well as its crystallographic orientation is inherited by rutile.
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spelling curtin-20.500.11937-210932017-09-13T13:46:02Z Processes of oxidation and HCl-leaching of Tellnes ilmenite Janssen, A. Putnis, Andrew Tellnes ilmenite is an important feedstock for the production of high-grade titanium pigment. The present study investigated the oxidation of ilmenite from Tellnes, Norway, at 700 °C in air and compared the leaching ability of pre-heated and non-heated Tellnes ilmenite in 20% HCl solution at 160 °C. Through the heat treatment, ilmenite (FeTiO3) is oxidized to hematite (Fe2O3) and rutile (TiO2) via a solid-state reaction mechanism. The leaching experiments revealed that after the pre-heating step the iron dissolution in the leaching process is limited due to the lower solubility of ferric iron in the hydrochloric acid. Furthermore, in both experiments the impurity phases such feldspar and orthopyroxene are less soluble in the hydrochloric acid and pollute the replacement product rutile because Si released from the impurity phases is incorporated in the rutile. The leaching reaction mechanism is interpreted as a pseudomorphic, interface-coupled dissolution-reprecipitation process, through which the external form of the parent ilmenite as well as its crystallographic orientation is inherited by rutile. 2011 Journal Article http://hdl.handle.net/20.500.11937/21093 10.1016/j.hydromet.2011.07.004 restricted
spellingShingle Janssen, A.
Putnis, Andrew
Processes of oxidation and HCl-leaching of Tellnes ilmenite
title Processes of oxidation and HCl-leaching of Tellnes ilmenite
title_full Processes of oxidation and HCl-leaching of Tellnes ilmenite
title_fullStr Processes of oxidation and HCl-leaching of Tellnes ilmenite
title_full_unstemmed Processes of oxidation and HCl-leaching of Tellnes ilmenite
title_short Processes of oxidation and HCl-leaching of Tellnes ilmenite
title_sort processes of oxidation and hcl-leaching of tellnes ilmenite
url http://hdl.handle.net/20.500.11937/21093