Promoted catalytic performances of highly dispersed V-doped SBA-16 catalysts for oxidative dehydrogenation of ethane to ethylene

© 2016. V-doped SBA-16 catalysts (V-SBA-16) with 3D nanocage mesopores have been successfully synthesized by a modified one-pot method under weak acid condition. The obtained materials were characterized by means of small angle XRD, N2 adsorption-desorption, TEM, UV-Vis and UV-Raman spectroscopy. Th...

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Main Authors: Kong, L., Li, J., Liu, Q., Zhao, Z., Sun, Q., Liu, Jian, Wei, Y.
Format: Journal Article
Published: Elsevier Inc. 2016
Online Access:http://hdl.handle.net/20.500.11937/19527
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author Kong, L.
Li, J.
Liu, Q.
Zhao, Z.
Sun, Q.
Liu, Jian
Wei, Y.
author_facet Kong, L.
Li, J.
Liu, Q.
Zhao, Z.
Sun, Q.
Liu, Jian
Wei, Y.
author_sort Kong, L.
building Curtin Institutional Repository
collection Online Access
description © 2016. V-doped SBA-16 catalysts (V-SBA-16) with 3D nanocage mesopores have been successfully synthesized by a modified one-pot method under weak acid condition. The obtained materials were characterized by means of small angle XRD, N2 adsorption-desorption, TEM, UV-Vis and UV-Raman spectroscopy. These characterization results indicated that well-order mesoporous structures were maintained even at higher vanadium loadings and high concentration of VO x species were incorporated into the framework of SBA-16 support. The catalytic performances of V-SBA-16, V/SBA-16 and V/SiO2 catalysts were comparatively investigated for the oxidative dehydrogenation of ethane to ethylene. The highest selectivity to ethylene of 63.3% and ethylene yield of 25.6% were obtained over 1.0V-SBA-16 catalyst. The superior catalytic performance of V-SBA-16 catalysts could be attributed to the presence of isolated framework VO x species, the unique structure of SBA-16 support and weak acidity. Moreover, V/SiO2 catalyst exhibited relatively poor catalytic activity duo to the formation of V2O5 nanoparticles on the surface of SiO2 support and the low dispersion of VO x species. These results indicated that the catalytic performances of the studied catalysts were strongly dependent on the vanadium loading, the nature and neighboring environment of VO x species and the structure of support.
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publishDate 2016
publisher Elsevier Inc.
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spelling curtin-20.500.11937-195272017-09-13T13:45:15Z Promoted catalytic performances of highly dispersed V-doped SBA-16 catalysts for oxidative dehydrogenation of ethane to ethylene Kong, L. Li, J. Liu, Q. Zhao, Z. Sun, Q. Liu, Jian Wei, Y. © 2016. V-doped SBA-16 catalysts (V-SBA-16) with 3D nanocage mesopores have been successfully synthesized by a modified one-pot method under weak acid condition. The obtained materials were characterized by means of small angle XRD, N2 adsorption-desorption, TEM, UV-Vis and UV-Raman spectroscopy. These characterization results indicated that well-order mesoporous structures were maintained even at higher vanadium loadings and high concentration of VO x species were incorporated into the framework of SBA-16 support. The catalytic performances of V-SBA-16, V/SBA-16 and V/SiO2 catalysts were comparatively investigated for the oxidative dehydrogenation of ethane to ethylene. The highest selectivity to ethylene of 63.3% and ethylene yield of 25.6% were obtained over 1.0V-SBA-16 catalyst. The superior catalytic performance of V-SBA-16 catalysts could be attributed to the presence of isolated framework VO x species, the unique structure of SBA-16 support and weak acidity. Moreover, V/SiO2 catalyst exhibited relatively poor catalytic activity duo to the formation of V2O5 nanoparticles on the surface of SiO2 support and the low dispersion of VO x species. These results indicated that the catalytic performances of the studied catalysts were strongly dependent on the vanadium loading, the nature and neighboring environment of VO x species and the structure of support. 2016 Journal Article http://hdl.handle.net/20.500.11937/19527 10.1016/j.jechem.2016.04.004 Elsevier Inc. restricted
spellingShingle Kong, L.
Li, J.
Liu, Q.
Zhao, Z.
Sun, Q.
Liu, Jian
Wei, Y.
Promoted catalytic performances of highly dispersed V-doped SBA-16 catalysts for oxidative dehydrogenation of ethane to ethylene
title Promoted catalytic performances of highly dispersed V-doped SBA-16 catalysts for oxidative dehydrogenation of ethane to ethylene
title_full Promoted catalytic performances of highly dispersed V-doped SBA-16 catalysts for oxidative dehydrogenation of ethane to ethylene
title_fullStr Promoted catalytic performances of highly dispersed V-doped SBA-16 catalysts for oxidative dehydrogenation of ethane to ethylene
title_full_unstemmed Promoted catalytic performances of highly dispersed V-doped SBA-16 catalysts for oxidative dehydrogenation of ethane to ethylene
title_short Promoted catalytic performances of highly dispersed V-doped SBA-16 catalysts for oxidative dehydrogenation of ethane to ethylene
title_sort promoted catalytic performances of highly dispersed v-doped sba-16 catalysts for oxidative dehydrogenation of ethane to ethylene
url http://hdl.handle.net/20.500.11937/19527