Tetracycline hydrochloride (TCH)-loaded drug carrier based on PLA:PCL nanofibre mats: experimental characterisation and release kinetics modelling

The experimental characterisation of electrospun poly(lactic acid) (PLA): poly(e-caprolactone) (PCL) as drug carriers, at five blend ratios from 1:0, 3:1, 1:1, 1:3 and 0:1, was holistically investigated in terms of their morphological structures, crystallinity levels and thermal properties. A widely...

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Main Authors: Haroosh, Hazim Jasim Mohammed, Dong, Yu, Lau, K.
Format: Journal Article
Published: Springer, Netherlands 2014
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/18870
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author Haroosh, Hazim Jasim Mohammed
Dong, Yu
Lau, K.
author_facet Haroosh, Hazim Jasim Mohammed
Dong, Yu
Lau, K.
author_sort Haroosh, Hazim Jasim Mohammed
building Curtin Institutional Repository
collection Online Access
description The experimental characterisation of electrospun poly(lactic acid) (PLA): poly(e-caprolactone) (PCL) as drug carriers, at five blend ratios from 1:0, 3:1, 1:1, 1:3 and 0:1, was holistically investigated in terms of their morphological structures, crystallinity levels and thermal properties. A widely used antibiotic tetracycline hydrochloride (TCH) was loaded to prepared fibrous mats at TCH concentrations of 1 and 5 wt%. The additional TCH into PLA: PCL better facilitates the reduction of fibre diameter than polymer blends. Increasing the TCH concentration from 1 to 5 wt% was found to result in only a modest decrease in the crystallinity level, but a significant increase in the crystallisation temperature (Tc) for PLA within PLA: PCL blends. The infrared spectra of fibre mats confirm the successful TCH encapsulation into fibrous networks. The first order and Zeng models for drug release kinetics were in better agreement with experimental release data, indicating the release acceleration of TCH with increasing its concentration. In a typical case of PLA: PCL (1:1) loaded with 5 wt% TCH, the fibre mats apparently demonstrate more wrinkled and floppy structures and increased fibre diameters and decreased inter-fibrous spaces after 7-day in vitro fibre degradation, as opposed to those obtained after 3-h degradation.
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format Journal Article
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institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T07:27:49Z
publishDate 2014
publisher Springer, Netherlands
recordtype eprints
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spelling curtin-20.500.11937-188702019-02-19T05:35:28Z Tetracycline hydrochloride (TCH)-loaded drug carrier based on PLA:PCL nanofibre mats: experimental characterisation and release kinetics modelling Haroosh, Hazim Jasim Mohammed Dong, Yu Lau, K. fibre technology characterization methods modelling The experimental characterisation of electrospun poly(lactic acid) (PLA): poly(e-caprolactone) (PCL) as drug carriers, at five blend ratios from 1:0, 3:1, 1:1, 1:3 and 0:1, was holistically investigated in terms of their morphological structures, crystallinity levels and thermal properties. A widely used antibiotic tetracycline hydrochloride (TCH) was loaded to prepared fibrous mats at TCH concentrations of 1 and 5 wt%. The additional TCH into PLA: PCL better facilitates the reduction of fibre diameter than polymer blends. Increasing the TCH concentration from 1 to 5 wt% was found to result in only a modest decrease in the crystallinity level, but a significant increase in the crystallisation temperature (Tc) for PLA within PLA: PCL blends. The infrared spectra of fibre mats confirm the successful TCH encapsulation into fibrous networks. The first order and Zeng models for drug release kinetics were in better agreement with experimental release data, indicating the release acceleration of TCH with increasing its concentration. In a typical case of PLA: PCL (1:1) loaded with 5 wt% TCH, the fibre mats apparently demonstrate more wrinkled and floppy structures and increased fibre diameters and decreased inter-fibrous spaces after 7-day in vitro fibre degradation, as opposed to those obtained after 3-h degradation. 2014 Journal Article http://hdl.handle.net/20.500.11937/18870 10.1007/s10853-014-8352-7 Springer, Netherlands fulltext
spellingShingle fibre technology
characterization methods
modelling
Haroosh, Hazim Jasim Mohammed
Dong, Yu
Lau, K.
Tetracycline hydrochloride (TCH)-loaded drug carrier based on PLA:PCL nanofibre mats: experimental characterisation and release kinetics modelling
title Tetracycline hydrochloride (TCH)-loaded drug carrier based on PLA:PCL nanofibre mats: experimental characterisation and release kinetics modelling
title_full Tetracycline hydrochloride (TCH)-loaded drug carrier based on PLA:PCL nanofibre mats: experimental characterisation and release kinetics modelling
title_fullStr Tetracycline hydrochloride (TCH)-loaded drug carrier based on PLA:PCL nanofibre mats: experimental characterisation and release kinetics modelling
title_full_unstemmed Tetracycline hydrochloride (TCH)-loaded drug carrier based on PLA:PCL nanofibre mats: experimental characterisation and release kinetics modelling
title_short Tetracycline hydrochloride (TCH)-loaded drug carrier based on PLA:PCL nanofibre mats: experimental characterisation and release kinetics modelling
title_sort tetracycline hydrochloride (tch)-loaded drug carrier based on pla:pcl nanofibre mats: experimental characterisation and release kinetics modelling
topic fibre technology
characterization methods
modelling
url http://hdl.handle.net/20.500.11937/18870