Effect of nitrogen-containing functionalization on the electrocatalytic activity of PtRu nanoparticles supported on carbon nanotubes for direct methanol fuel cells

PtRu nanoparticles (NPs) with average size of ∼3 nm are supported onto poly(diallyldimethylammonium chloride) (PDDA), polyethylenimine (PEI), 1-aminopyrene (1-AP or AP), and terahydrofuran (THF) functionalized multi-walled carbon nanotubes (CNTs) using microwave assisted self-assembly method. The Pt...

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Main Authors: Cheng, Yi, Xu, C., Shen, P., Jiang, San Ping
Format: Journal Article
Published: elsevier 2014
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/18272
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author Cheng, Yi
Xu, C.
Shen, P.
Jiang, San Ping
author_facet Cheng, Yi
Xu, C.
Shen, P.
Jiang, San Ping
author_sort Cheng, Yi
building Curtin Institutional Repository
collection Online Access
description PtRu nanoparticles (NPs) with average size of ∼3 nm are supported onto poly(diallyldimethylammonium chloride) (PDDA), polyethylenimine (PEI), 1-aminopyrene (1-AP or AP), and terahydrofuran (THF) functionalized multi-walled carbon nanotubes (CNTs) using microwave assisted self-assembly method. The PtRu/CNTs catalysts are extensively characterized by TGA, TEM, XRD, XPS, cyclic voltammetry and chronoamperometry. Non-covalent functionalization substantially improves the dispersion and distribution of PtRu NPs on CNTs. Most important, the results demonstrate that nitrogen-containing functional groups of the functionalization agents play a critical role in the electrocatalystic activity of PtRu NPs supported on CNTs. PtRu NPs supported on PEI, AP and in less extent PDDA functionalized CNTs exhibited significantly higher electrocatalystic activity and stability for the electro-oxidation of methanol as compared with PtRu supported on THF-CNTs and conventional acid-treated CNTs. The superior activity of PtRu supported on functionalized CNTs is most likely due to the strong interaction of the electron rich nitrogen-containing functional groups of the functionalization agents such as PEI, AP and in less extend PDDA and the PtRu NPs assembled on CNTs.
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institution Curtin University Malaysia
institution_category Local University
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publishDate 2014
publisher elsevier
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spelling curtin-20.500.11937-182722017-09-13T15:57:25Z Effect of nitrogen-containing functionalization on the electrocatalytic activity of PtRu nanoparticles supported on carbon nanotubes for direct methanol fuel cells Cheng, Yi Xu, C. Shen, P. Jiang, San Ping reaction Nitrogen-containing Fuel cells Methanol oxidation Solvent functionalization Polyelectrolyte PtRu nanoparticles PtRu nanoparticles (NPs) with average size of ∼3 nm are supported onto poly(diallyldimethylammonium chloride) (PDDA), polyethylenimine (PEI), 1-aminopyrene (1-AP or AP), and terahydrofuran (THF) functionalized multi-walled carbon nanotubes (CNTs) using microwave assisted self-assembly method. The PtRu/CNTs catalysts are extensively characterized by TGA, TEM, XRD, XPS, cyclic voltammetry and chronoamperometry. Non-covalent functionalization substantially improves the dispersion and distribution of PtRu NPs on CNTs. Most important, the results demonstrate that nitrogen-containing functional groups of the functionalization agents play a critical role in the electrocatalystic activity of PtRu NPs supported on CNTs. PtRu NPs supported on PEI, AP and in less extent PDDA functionalized CNTs exhibited significantly higher electrocatalystic activity and stability for the electro-oxidation of methanol as compared with PtRu supported on THF-CNTs and conventional acid-treated CNTs. The superior activity of PtRu supported on functionalized CNTs is most likely due to the strong interaction of the electron rich nitrogen-containing functional groups of the functionalization agents such as PEI, AP and in less extend PDDA and the PtRu NPs assembled on CNTs. 2014 Journal Article http://hdl.handle.net/20.500.11937/18272 10.1016/j.apcatb.2014.04.017 elsevier restricted
spellingShingle reaction
Nitrogen-containing
Fuel cells
Methanol oxidation
Solvent
functionalization
Polyelectrolyte
PtRu nanoparticles
Cheng, Yi
Xu, C.
Shen, P.
Jiang, San Ping
Effect of nitrogen-containing functionalization on the electrocatalytic activity of PtRu nanoparticles supported on carbon nanotubes for direct methanol fuel cells
title Effect of nitrogen-containing functionalization on the electrocatalytic activity of PtRu nanoparticles supported on carbon nanotubes for direct methanol fuel cells
title_full Effect of nitrogen-containing functionalization on the electrocatalytic activity of PtRu nanoparticles supported on carbon nanotubes for direct methanol fuel cells
title_fullStr Effect of nitrogen-containing functionalization on the electrocatalytic activity of PtRu nanoparticles supported on carbon nanotubes for direct methanol fuel cells
title_full_unstemmed Effect of nitrogen-containing functionalization on the electrocatalytic activity of PtRu nanoparticles supported on carbon nanotubes for direct methanol fuel cells
title_short Effect of nitrogen-containing functionalization on the electrocatalytic activity of PtRu nanoparticles supported on carbon nanotubes for direct methanol fuel cells
title_sort effect of nitrogen-containing functionalization on the electrocatalytic activity of ptru nanoparticles supported on carbon nanotubes for direct methanol fuel cells
topic reaction
Nitrogen-containing
Fuel cells
Methanol oxidation
Solvent
functionalization
Polyelectrolyte
PtRu nanoparticles
url http://hdl.handle.net/20.500.11937/18272