Correlation between proton conductivity, thermal stability and structural symmetries in novel HPW-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells

The intrinsic relationship between proton conductivity, thermal stability and structural symmetries of phosphotungstic acid (HPW)-functionalized mesoporous silica (HPW-meso-silica) membrane was investigated with mesoporous silica from 2D hexagonal p6mm, 3D face-centered cubic (Fm¯3m), body-centered...

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Main Authors: Zeng, J., Shen, P., Lu, S., Xiang, Y., Li, L., De Marco, Roland, Jiang, San Ping
Format: Journal Article
Published: Elsevier B.V 2012
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/17287
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author Zeng, J.
Shen, P.
Lu, S.
Xiang, Y.
Li, L.
De Marco, Roland
Jiang, San Ping
author_facet Zeng, J.
Shen, P.
Lu, S.
Xiang, Y.
Li, L.
De Marco, Roland
Jiang, San Ping
author_sort Zeng, J.
building Curtin Institutional Repository
collection Online Access
description The intrinsic relationship between proton conductivity, thermal stability and structural symmetries of phosphotungstic acid (HPW)-functionalized mesoporous silica (HPW-meso-silica) membrane was investigated with mesoporous silica from 2D hexagonal p6mm, 3D face-centered cubic (Fm¯3m), body-centered Im¯3m, to cubic bicontinuous Ia¯3d symmetries. HPW-meso-silica nanocomposites with 3D mesostructures display a significantly higher proton conductivity and higher stability as a function of relative humidity in comparison to 2D mesostructures. The best result was obtained with body-centered cubic (Im¯3m)-HPWmeso-silica, showing proton conductivities of 0.061 S cm-1 at 25°C and 0.14 S cm-1 at 150°C, respectively, and an activation energy of 10.0 kJ mol-1. At 150°C, the cell employing a HPW-meso-silica membrane produced a maximum power output of 237 mW cm-2 in a methanol fuel without external humidification. The high proton conductivity and excellent performance of the new methanol fuel cells demonstrate the promise of HPW-meso-silica nanocomposites with 3D mesostructures as a new class of inorganic proton exchange membranes for use in direct methanol fuel cells (DMFCs).
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institution Curtin University Malaysia
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publishDate 2012
publisher Elsevier B.V
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spelling curtin-20.500.11937-172872017-09-13T15:43:05Z Correlation between proton conductivity, thermal stability and structural symmetries in novel HPW-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells Zeng, J. Shen, P. Lu, S. Xiang, Y. Li, L. De Marco, Roland Jiang, San Ping High temperature proton exchange membranes Structural symmetries Mesoporous silica Direct methanol fuel cells Heteropolyacid The intrinsic relationship between proton conductivity, thermal stability and structural symmetries of phosphotungstic acid (HPW)-functionalized mesoporous silica (HPW-meso-silica) membrane was investigated with mesoporous silica from 2D hexagonal p6mm, 3D face-centered cubic (Fm¯3m), body-centered Im¯3m, to cubic bicontinuous Ia¯3d symmetries. HPW-meso-silica nanocomposites with 3D mesostructures display a significantly higher proton conductivity and higher stability as a function of relative humidity in comparison to 2D mesostructures. The best result was obtained with body-centered cubic (Im¯3m)-HPWmeso-silica, showing proton conductivities of 0.061 S cm-1 at 25°C and 0.14 S cm-1 at 150°C, respectively, and an activation energy of 10.0 kJ mol-1. At 150°C, the cell employing a HPW-meso-silica membrane produced a maximum power output of 237 mW cm-2 in a methanol fuel without external humidification. The high proton conductivity and excellent performance of the new methanol fuel cells demonstrate the promise of HPW-meso-silica nanocomposites with 3D mesostructures as a new class of inorganic proton exchange membranes for use in direct methanol fuel cells (DMFCs). 2012 Journal Article http://hdl.handle.net/20.500.11937/17287 10.1016/j.memsci.2012.01.018 Elsevier B.V restricted
spellingShingle High temperature proton exchange membranes
Structural symmetries
Mesoporous silica
Direct methanol fuel cells
Heteropolyacid
Zeng, J.
Shen, P.
Lu, S.
Xiang, Y.
Li, L.
De Marco, Roland
Jiang, San Ping
Correlation between proton conductivity, thermal stability and structural symmetries in novel HPW-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells
title Correlation between proton conductivity, thermal stability and structural symmetries in novel HPW-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells
title_full Correlation between proton conductivity, thermal stability and structural symmetries in novel HPW-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells
title_fullStr Correlation between proton conductivity, thermal stability and structural symmetries in novel HPW-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells
title_full_unstemmed Correlation between proton conductivity, thermal stability and structural symmetries in novel HPW-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells
title_short Correlation between proton conductivity, thermal stability and structural symmetries in novel HPW-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells
title_sort correlation between proton conductivity, thermal stability and structural symmetries in novel hpw-meso-silica nanocomposite membranes and their performance in direct methanol fuel cells
topic High temperature proton exchange membranes
Structural symmetries
Mesoporous silica
Direct methanol fuel cells
Heteropolyacid
url http://hdl.handle.net/20.500.11937/17287