Synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide

The coordination chemistry of amide-substituted calixarenes is reviewed. The synthesis of a gadolinium complex of a trisamide calix[4]arene is described, involving the reaction of 5,11,17,23-tetra-tert-butyl-24-hydroxy-26,27,28-tris(diethylcarbamoylmethoxy) calix[4]arene (L) with gadolinium picrate...

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Main Authors: Ogden, Mark, Skelton, B., White, A.
Format: Journal Article
Published: Elsevier SAS 2005
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/17105
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author Ogden, Mark
Skelton, B.
White, A.
author_facet Ogden, Mark
Skelton, B.
White, A.
author_sort Ogden, Mark
building Curtin Institutional Repository
collection Online Access
description The coordination chemistry of amide-substituted calixarenes is reviewed. The synthesis of a gadolinium complex of a trisamide calix[4]arene is described, involving the reaction of 5,11,17,23-tetra-tert-butyl-24-hydroxy-26,27,28-tris(diethylcarbamoylmethoxy) calix[4]arene (L) with gadolinium picrate dodecahydrate. Structural studies demonstrated that the complex can be formulated as [(pic-O)Gd{(L H)(EtOH)}](pic)2 EtOH.
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spelling curtin-20.500.11937-171052017-09-13T15:43:55Z Synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide Ogden, Mark Skelton, B. White, A. Lanthanide Calixarene Crystal structure Picrate The coordination chemistry of amide-substituted calixarenes is reviewed. The synthesis of a gadolinium complex of a trisamide calix[4]arene is described, involving the reaction of 5,11,17,23-tetra-tert-butyl-24-hydroxy-26,27,28-tris(diethylcarbamoylmethoxy) calix[4]arene (L) with gadolinium picrate dodecahydrate. Structural studies demonstrated that the complex can be formulated as [(pic-O)Gd{(L H)(EtOH)}](pic)2 EtOH. 2005 Journal Article http://hdl.handle.net/20.500.11937/17105 10.1016/j.crci.2004.10.019 Elsevier SAS fulltext
spellingShingle Lanthanide
Calixarene
Crystal structure
Picrate
Ogden, Mark
Skelton, B.
White, A.
Synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide
title Synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide
title_full Synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide
title_fullStr Synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide
title_full_unstemmed Synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide
title_short Synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide
title_sort synthesis and structural studies of a lanthanide complex of a calix[4]arene tris-amide
topic Lanthanide
Calixarene
Crystal structure
Picrate
url http://hdl.handle.net/20.500.11937/17105