WaMn1 - aox Catalysts Synthesized by a One-Step Urea Co-precipitation Method for Selective Catalytic Reduction of NOx with NH3 at Low Temperatures

Selective catalytic reduction (SCR) of NOx with NH3 (NH3-SCR) at low temperatures is a promising technology for DeNOx (removal of NOx) as a result of its high NOx conversion, excellent selectivity, and broad application prospect. As a result of the remarkable activity under low temperature for SCR p...

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Main Authors: Sun, W., Li, Xin Yong, Zhao, Q., Tade, M., Liu, Shaomin
Format: Journal Article
Published: American Chemical Society 2016
Online Access:http://hdl.handle.net/20.500.11937/14862
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author Sun, W.
Li, Xin Yong
Zhao, Q.
Tade, M.
Liu, Shaomin
author_facet Sun, W.
Li, Xin Yong
Zhao, Q.
Tade, M.
Liu, Shaomin
author_sort Sun, W.
building Curtin Institutional Repository
collection Online Access
description Selective catalytic reduction (SCR) of NOx with NH3 (NH3-SCR) at low temperatures is a promising technology for DeNOx (removal of NOx) as a result of its high NOx conversion, excellent selectivity, and broad application prospect. As a result of the remarkable activity under low temperature for SCR performance, Mn-based catalysts have attracted extensive attention. In this work, a series of WαMn1 – αOx (α = 0, 0.25, 0.33, 0.5, or 1) catalysts were synthesized by a one-step urea co-precipitation method and characterized by X-ray diffraction, Raman, X-ray photoelectron spectroscopy, thermogravimetric analysis, and scanning electron microscopy. Thereamong, the W0.33Mn0.66Ox catalyst showed the highest NH3-SCR activity within a broad temperature range of 230–470 °C. In addition, the active Mn and W species were in highly amorphous or poorly crystalline states. It was revealed that the interaction of W and Mn increased the chemistry oxygen content of the catalysts, thus enhancing the low-temperature SCR performance.
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institution Curtin University Malaysia
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spelling curtin-20.500.11937-148622017-09-13T15:02:13Z WaMn1 - aox Catalysts Synthesized by a One-Step Urea Co-precipitation Method for Selective Catalytic Reduction of NOx with NH3 at Low Temperatures Sun, W. Li, Xin Yong Zhao, Q. Tade, M. Liu, Shaomin Selective catalytic reduction (SCR) of NOx with NH3 (NH3-SCR) at low temperatures is a promising technology for DeNOx (removal of NOx) as a result of its high NOx conversion, excellent selectivity, and broad application prospect. As a result of the remarkable activity under low temperature for SCR performance, Mn-based catalysts have attracted extensive attention. In this work, a series of WαMn1 – αOx (α = 0, 0.25, 0.33, 0.5, or 1) catalysts were synthesized by a one-step urea co-precipitation method and characterized by X-ray diffraction, Raman, X-ray photoelectron spectroscopy, thermogravimetric analysis, and scanning electron microscopy. Thereamong, the W0.33Mn0.66Ox catalyst showed the highest NH3-SCR activity within a broad temperature range of 230–470 °C. In addition, the active Mn and W species were in highly amorphous or poorly crystalline states. It was revealed that the interaction of W and Mn increased the chemistry oxygen content of the catalysts, thus enhancing the low-temperature SCR performance. 2016 Journal Article http://hdl.handle.net/20.500.11937/14862 10.1021/acs.energyfuels.5b02252 American Chemical Society restricted
spellingShingle Sun, W.
Li, Xin Yong
Zhao, Q.
Tade, M.
Liu, Shaomin
WaMn1 - aox Catalysts Synthesized by a One-Step Urea Co-precipitation Method for Selective Catalytic Reduction of NOx with NH3 at Low Temperatures
title WaMn1 - aox Catalysts Synthesized by a One-Step Urea Co-precipitation Method for Selective Catalytic Reduction of NOx with NH3 at Low Temperatures
title_full WaMn1 - aox Catalysts Synthesized by a One-Step Urea Co-precipitation Method for Selective Catalytic Reduction of NOx with NH3 at Low Temperatures
title_fullStr WaMn1 - aox Catalysts Synthesized by a One-Step Urea Co-precipitation Method for Selective Catalytic Reduction of NOx with NH3 at Low Temperatures
title_full_unstemmed WaMn1 - aox Catalysts Synthesized by a One-Step Urea Co-precipitation Method for Selective Catalytic Reduction of NOx with NH3 at Low Temperatures
title_short WaMn1 - aox Catalysts Synthesized by a One-Step Urea Co-precipitation Method for Selective Catalytic Reduction of NOx with NH3 at Low Temperatures
title_sort wamn1 - aox catalysts synthesized by a one-step urea co-precipitation method for selective catalytic reduction of nox with nh3 at low temperatures
url http://hdl.handle.net/20.500.11937/14862