Synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine

From the reaction of biguanide with ethyl benzoylacetate, N-(6-oxo-4-phenyl-1,6-dihydropyrimidin-2-yl)guanidine and 6-benzoylmethyl-1,3,5-triazin-2,4-diamine were isolated.The structural evaluation of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine was performed theoretically (DFT calculations) and experi...

Full description

Bibliographic Details
Main Authors: Sachdeva, N., Dolzhenko, Anton, Chui, W.
Format: Journal Article
Published: Elsevier SAS 2011
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/14796
_version_ 1848748718857125888
author Sachdeva, N.
Dolzhenko, Anton
Chui, W.
author_facet Sachdeva, N.
Dolzhenko, Anton
Chui, W.
author_sort Sachdeva, N.
building Curtin Institutional Repository
collection Online Access
description From the reaction of biguanide with ethyl benzoylacetate, N-(6-oxo-4-phenyl-1,6-dihydropyrimidin-2-yl)guanidine and 6-benzoylmethyl-1,3,5-triazin-2,4-diamine were isolated.The structural evaluation of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine was performed theoretically (DFT calculations) and experimentally (NMR spectroscopy and X-ray crystallography). The effects of solvents and temperature on keto-enol-enaminone tautomeric equilibrium were explored.
first_indexed 2025-11-14T07:09:30Z
format Journal Article
id curtin-20.500.11937-14796
institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T07:09:30Z
publishDate 2011
publisher Elsevier SAS
recordtype eprints
repository_type Digital Repository
spelling curtin-20.500.11937-147962017-09-13T15:54:45Z Synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine Sachdeva, N. Dolzhenko, Anton Chui, W. X-ray crystal structure Solvent effect DFT calculations Triazines Tautomerism Resonance-assisted hydrogenbonding From the reaction of biguanide with ethyl benzoylacetate, N-(6-oxo-4-phenyl-1,6-dihydropyrimidin-2-yl)guanidine and 6-benzoylmethyl-1,3,5-triazin-2,4-diamine were isolated.The structural evaluation of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine was performed theoretically (DFT calculations) and experimentally (NMR spectroscopy and X-ray crystallography). The effects of solvents and temperature on keto-enol-enaminone tautomeric equilibrium were explored. 2011 Journal Article http://hdl.handle.net/20.500.11937/14796 10.1016/j.crci.2010.10.003 Elsevier SAS restricted
spellingShingle X-ray crystal structure
Solvent effect
DFT calculations
Triazines
Tautomerism
Resonance-assisted hydrogenbonding
Sachdeva, N.
Dolzhenko, Anton
Chui, W.
Synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine
title Synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine
title_full Synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine
title_fullStr Synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine
title_full_unstemmed Synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine
title_short Synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine
title_sort synthesis and tautomerism study of 6-benzoylmethyl-1,3,5-triazin-2,4-diamine
topic X-ray crystal structure
Solvent effect
DFT calculations
Triazines
Tautomerism
Resonance-assisted hydrogenbonding
url http://hdl.handle.net/20.500.11937/14796