Formation of Aromatic Structures during the Pyrolysis of Bio-oil

The pyrolysis of biomass to produce bio-oil is a very effective way of biomass use. Bio-oil undergoes drastic structural changes as it is upgraded into biofuels or used as a fuel for gasification/combustion. The evolution of aromatic ring systems in bio-oil is a key consideration in bio-oil use. A b...

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Main Authors: Wang, Yi, Li, X., Mourant, Daniel, Gunawan, Richard, Zhang, Shu, Li, Chun-Zhu
Format: Journal Article
Published: American Chemical Society 2012
Online Access:http://hdl.handle.net/20.500.11937/14020
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author Wang, Yi
Li, X.
Mourant, Daniel
Gunawan, Richard
Zhang, Shu
Li, Chun-Zhu
author_facet Wang, Yi
Li, X.
Mourant, Daniel
Gunawan, Richard
Zhang, Shu
Li, Chun-Zhu
author_sort Wang, Yi
building Curtin Institutional Repository
collection Online Access
description The pyrolysis of biomass to produce bio-oil is a very effective way of biomass use. Bio-oil undergoes drastic structural changes as it is upgraded into biofuels or used as a fuel for gasification/combustion. The evolution of aromatic ring systems in bio-oil is a key consideration in bio-oil use. A bio-oil sample produced from the fast pyrolysis of mallee wood at 500 °C, its lignin-derived oligomers, and pure cellulose have been pyrolyzed in a novel two-stage fluidized-bed/fixed-bed reactor at temperatures between 350 and 850 °C. The product tars were characterized with ultraviolet (UV) fluorescence spectroscopy. Our results indicate that significant portions of aromatic ring systems in the bio-oil could turn/polymerize into solids not soluble in CHCl3 + CH3OH during the pyrolysis at relatively low temperatures, e.g., 350–400 °C. This process can be enhanced by the presence of cellulose-/hemicellulose-derived species in the bio-oil, which are reactive and produce radicals to enhance the polymerization reactions. The pyrolysis of cellulose-derived species in the bio-oil tended to form additional very large aromatic ring systems at temperatures higher than 700 °C.
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institution Curtin University Malaysia
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publishDate 2012
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spelling curtin-20.500.11937-140202017-09-13T14:04:52Z Formation of Aromatic Structures during the Pyrolysis of Bio-oil Wang, Yi Li, X. Mourant, Daniel Gunawan, Richard Zhang, Shu Li, Chun-Zhu The pyrolysis of biomass to produce bio-oil is a very effective way of biomass use. Bio-oil undergoes drastic structural changes as it is upgraded into biofuels or used as a fuel for gasification/combustion. The evolution of aromatic ring systems in bio-oil is a key consideration in bio-oil use. A bio-oil sample produced from the fast pyrolysis of mallee wood at 500 °C, its lignin-derived oligomers, and pure cellulose have been pyrolyzed in a novel two-stage fluidized-bed/fixed-bed reactor at temperatures between 350 and 850 °C. The product tars were characterized with ultraviolet (UV) fluorescence spectroscopy. Our results indicate that significant portions of aromatic ring systems in the bio-oil could turn/polymerize into solids not soluble in CHCl3 + CH3OH during the pyrolysis at relatively low temperatures, e.g., 350–400 °C. This process can be enhanced by the presence of cellulose-/hemicellulose-derived species in the bio-oil, which are reactive and produce radicals to enhance the polymerization reactions. The pyrolysis of cellulose-derived species in the bio-oil tended to form additional very large aromatic ring systems at temperatures higher than 700 °C. 2012 Journal Article http://hdl.handle.net/20.500.11937/14020 10.1021/ef201155e American Chemical Society restricted
spellingShingle Wang, Yi
Li, X.
Mourant, Daniel
Gunawan, Richard
Zhang, Shu
Li, Chun-Zhu
Formation of Aromatic Structures during the Pyrolysis of Bio-oil
title Formation of Aromatic Structures during the Pyrolysis of Bio-oil
title_full Formation of Aromatic Structures during the Pyrolysis of Bio-oil
title_fullStr Formation of Aromatic Structures during the Pyrolysis of Bio-oil
title_full_unstemmed Formation of Aromatic Structures during the Pyrolysis of Bio-oil
title_short Formation of Aromatic Structures during the Pyrolysis of Bio-oil
title_sort formation of aromatic structures during the pyrolysis of bio-oil
url http://hdl.handle.net/20.500.11937/14020