The aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions

This paper presents a theoretical investigation on the ionic equilibrium of Fe(III)-Ni(II)-H2SO4-H2O system. A non-ideal speciation model is developed to calculate the concentration distribution of iron and nickel species in a mixed ferric and nickel sulphate aqueous solution over the pH range from...

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Main Authors: Wang, K., Li, J., McDonald, R., Browner, R.
Other Authors: Pradip - president
Format: Conference Paper
Published: IMPC 2012
Subjects:
Online Access:http://hdl.handle.net/20.500.11937/11727
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author Wang, K.
Li, J.
McDonald, R.
Browner, R.
author2 Pradip - president
author_facet Pradip - president
Wang, K.
Li, J.
McDonald, R.
Browner, R.
author_sort Wang, K.
building Curtin Institutional Repository
collection Online Access
description This paper presents a theoretical investigation on the ionic equilibrium of Fe(III)-Ni(II)-H2SO4-H2O system. A non-ideal speciation model is developed to calculate the concentration distribution of iron and nickel species in a mixed ferric and nickel sulphate aqueous solution over the pH range from 0 to 4 and temperature from 25 to 100°C. A series of speciation diagrams for iron and nickel species is plotted with the effects of ionic strength and temperature on the equilibrium constants being taken into account. The ionic strength-dependent equilibrium constant is treated through a semi-empirical Vasil'eV equation, which is based on an extended Debye-Hückel theory. A Helgeson model is applied to extrapolate the equilibrium constant to elevated temperature. The ionic equilibrium reactions are described by a group of numerical equations containing the temperature and ionic strength-dependent equilibrium constants, which are solved by the Newton-Raphson method. The speciation model is also applied to estimate the hydrogen ion activities and corresponding pH values. The calculated pH values are in agreement with the experimentally measured pH, and are compared to literature data and pH values produced by the Visual MINTEQ® program (a computer code for the calculation of chemical equilibrium in natural aqueous system). This investigation provides a deep insight into the ionic equilibrium behavior of a mixed metal sulphate aqueous system which commonly occurs in hydrometallurgical processing.
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institution Curtin University Malaysia
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publishDate 2012
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spelling curtin-20.500.11937-117272017-02-28T01:33:14Z The aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions Wang, K. Li, J. McDonald, R. Browner, R. Pradip - president Speciation Chemical modelling Parker CRC Thermodynamics Nickel Iron This paper presents a theoretical investigation on the ionic equilibrium of Fe(III)-Ni(II)-H2SO4-H2O system. A non-ideal speciation model is developed to calculate the concentration distribution of iron and nickel species in a mixed ferric and nickel sulphate aqueous solution over the pH range from 0 to 4 and temperature from 25 to 100°C. A series of speciation diagrams for iron and nickel species is plotted with the effects of ionic strength and temperature on the equilibrium constants being taken into account. The ionic strength-dependent equilibrium constant is treated through a semi-empirical Vasil'eV equation, which is based on an extended Debye-Hückel theory. A Helgeson model is applied to extrapolate the equilibrium constant to elevated temperature. The ionic equilibrium reactions are described by a group of numerical equations containing the temperature and ionic strength-dependent equilibrium constants, which are solved by the Newton-Raphson method. The speciation model is also applied to estimate the hydrogen ion activities and corresponding pH values. The calculated pH values are in agreement with the experimentally measured pH, and are compared to literature data and pH values produced by the Visual MINTEQ® program (a computer code for the calculation of chemical equilibrium in natural aqueous system). This investigation provides a deep insight into the ionic equilibrium behavior of a mixed metal sulphate aqueous system which commonly occurs in hydrometallurgical processing. 2012 Conference Paper http://hdl.handle.net/20.500.11937/11727 IMPC restricted
spellingShingle Speciation
Chemical modelling
Parker CRC
Thermodynamics
Nickel
Iron
Wang, K.
Li, J.
McDonald, R.
Browner, R.
The aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions
title The aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions
title_full The aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions
title_fullStr The aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions
title_full_unstemmed The aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions
title_short The aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions
title_sort aqueous ionic equilibrium and speciation of iron and nickel in sulphuric solutions
topic Speciation
Chemical modelling
Parker CRC
Thermodynamics
Nickel
Iron
url http://hdl.handle.net/20.500.11937/11727